2-(6-(3-(trifluoromethoxy)benzyloxy)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetic acid trifluoroacetate

Base Information

Chemical Name:2-(6-(3-(trifluoromethoxy)benzyloxy)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetic acid trifluoroacetate
CAS No.:1262007-40-8
Molecular Formula:C₂₁H₁₉F₃N₂O₄
Molecular Weight:420.388
Hs Code.:

Synonyms:2-(6-(3-(trifluoromethoxy)benzyloxy)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetic acid trifluoroacetate

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Chemical Property of 2-(6-(3-(trifluoromethoxy)benzyloxy)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetic acid trifluoroacetate

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Technology Process of 2-(6-(3-(trifluoromethoxy)benzyloxy)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetic acid trifluoroacetate

There total 6 articles about 2-(6-(3-(trifluoromethoxy)benzyloxy)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetic acid trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₂₉F₃N₂O₆

: 1262007-40-8
2-(6-(3-(trifluoromethoxy)benzyloxy)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetic acid trifluoroacetate

Guidance literature:: C₂₇H₂₉F₃N₂O₆; With lithium hydroxide; In 1,4-dioxane;

With hydrogenchloride; In 1,4-dioxane; water; for 1h;

Reference yield:

: 52055-23-9
5-benzyloxytryptamine hydrochloride

: 1262007-40-8
2-(6-(3-(trifluoromethoxy)benzyloxy)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetic acid trifluoroacetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid; water / methanol / 80 °C

2.1: hydrogen / 10% palladium on activated charcoal / tetrahydrofuran; methanol / 1 h / 20 °C

3.1: triethylamine / 1,4-dioxane / 2 h / 20 °C

4.1: caesium carbonate / N,N-dimethyl-formamide / 60 °C

5.1: lithium hydroxide / 1,4-dioxane

5.2: 1 h

With water; hydrogen; caesium carbonate; triethylamine; trifluoroacetic acid; lithium hydroxide; 10% palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;

Reference yield:

: 1262007-84-0
methyl 2-(6-(benzyloxy)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetate

: 1262007-40-8
2-(6-(3-(trifluoromethoxy)benzyloxy)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetic acid trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / 10% palladium on activated charcoal / tetrahydrofuran; methanol / 1 h / 20 °C

2.1: triethylamine / 1,4-dioxane / 2 h / 20 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 60 °C

4.1: lithium hydroxide / 1,4-dioxane

4.2: 1 h

With hydrogen; caesium carbonate; triethylamine; lithium hydroxide; 10% palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;