Technology Process of C22H28O7S
There total 5 articles about C22H28O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap;
In
pyridine;
at 20 ℃;
for 24h;
regioselective reaction;
DOI:10.1002/asia.201000602
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium borohydride / tetrahydrofuran / 6 h / 20 °C
2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C
3: water; acetic acid / 48 h / 20 °C
4: dmap / pyridine / 24 h / 20 °C
With
dmap; lithium borohydride; sodium hydride;
In
tetrahydrofuran; pyridine; water; acetic acid; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/asia.201000602
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C
2: water; acetic acid / 48 h / 20 °C
3: dmap / pyridine / 24 h / 20 °C
With
dmap; sodium hydride;
In
pyridine; water; acetic acid; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/asia.201000602