METHYL-2,3,4-TRI-O-ACETYL-BETA-D-GALACTOPYRANOSYLURONOSYL AZIDE

Base Information

Chemical Name:METHYL-2,3,4-TRI-O-ACETYL-BETA-D-GALACTOPYRANOSYLURONOSYL AZIDE
CAS No.:163776-36-1
Molecular Formula:C₁₃H₁₇N₃O₉
Molecular Weight:359.293
Hs Code.:
Mol file:163776-36-1.mol

Synonyms:METHYL-2,3,4-TRI-O-ACETYL-BETA-D-GALACTOPYRANOSYLURONOSYL AZIDE;METHYL-2,3,4-TRI-O-ACETYL-SS-D-GALACTOPYRANOSYLURONOSYL AZIDE

Suppliers and Price of METHYL-2,3,4-TRI-O-ACETYL-BETA-D-GALACTOPYRANOSYLURONOSYL AZIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of METHYL-2,3,4-TRI-O-ACETYL-BETA-D-GALACTOPYRANOSYLURONOSYL AZIDE

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of METHYL-2,3,4-TRI-O-ACETYL-BETA-D-GALACTOPYRANOSYLURONOSYL AZIDE

There total 42 articles about METHYL-2,3,4-TRI-O-ACETYL-BETA-D-GALACTOPYRANOSYLURONOSYL AZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 7355-18-2
(2S,3S,4S,5R,6S)-3,4,5,6-Tetraacetoxy-tetrahydro-pyran-2-carboxylic acid methyl ester

: 67776-38-9,163776-36-1
2,3,4-tri-O-acetyl-1-azido-1-deoxy-β-D-glucopyranuronic acid methyl ester

Guidance literature:: With trimethylsilylazide; tin(IV) chloride; In dichloromethane; for 15h;
DOI:10.1021/ol026629j

Reference yield: 93.0%

: 163776-36-1
methyl (2,3,4-tri-O-acetyl-β-D-galactopyranosyl azide)uronate

: 163776-36-1
methyl 2,3,4-tri-O-acetyl-1-azido-1-deoxy-α-D-galactopyranuronate

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -18 - -15 ℃; for 48h; stereoselective reaction;
DOI:10.1002/chem.201302572

Reference yield: 92.0%

: 21085-72-3
1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester

: 67776-38-9,163776-36-1
2,3,4-tri-O-acetyl-1-azido-1-deoxy-β-D-glucopyranuronic acid methyl ester

Guidance literature:: With sodium azide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; sodium hydrogencarbonate; at 20 ℃; for 2h;
DOI:10.1016/S0008-6215(00)00228-7