C₁₈H₂₂N₂O₃Se

Base Information

• Chemical Name: C₁₈H₂₂N₂O₃Se
• CAS No.: 1315303-30-0
• Molecular Formula: C₁₈H₂₂N₂O₃Se
• Molecular Weight: 393.344
• Mol file: 1315303-30-0.mol

Synonyms:C₁₈H₂₂N₂O₃Se

Chemical Property of C₁₈H₂₂N₂O₃Se

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₂₂N₂O₃Se

There total 4 articles about C₁₈H₂₂N₂O₃Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

dibutyl diselenide (20333-40-8) + C14H13BrN2O3 (1315303-29-7) → C18H22N2O3Se (1315303-30-0)

Guidance literature:

dibutyl diselenide; With sodium tetrahydroborate; In ethanol; at 0 - 20 ℃; for 0.5h;

C₁₄H₁₃BrN₂O₃; In ethanol; at 20 ℃; for 4h;

DOI:10.1039/c1cc12152a

Reference yield:

C14H11BrN2O3 (1315303-28-6) → C18H22N2O3Se (1315303-30-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / ethanol / 6 h / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate / ethanol / 0.5 h / 0 - 20 °C

2.2: 4 h / 20 °C

With sodium tetrahydroborate; In ethanol;

DOI:10.1039/c1cc12152a

Reference yield:

4-methoxy-aniline (104-94-9) → C18H22N2O3Se (1315303-30-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: acetic acid / 20 °C

2.1: sodium tetrahydroborate / ethanol / 6 h / 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate / ethanol / 0.5 h / 0 - 20 °C

3.2: 4 h / 20 °C

With sodium tetrahydroborate; acetic acid; In ethanol;

DOI:10.1039/c1cc12152a

upstream raw materials:

C₁₄H₁₁BrN₂O₃

dibutyl diselenide

C₁₄H₁₃BrN₂O₃

4-methoxy-aniline

Downstream raw materials:

C₂₈H₂₀N₄O₆Se₂