C₂₄H₂₆ClF₃N₄O

Base Information

Chemical Name:C₂₄H₂₆ClF₃N₄O
CAS No.:1037361-22-0
Molecular Formula:C₂₄H₂₆ClF₃N₄O
Molecular Weight:478.945
Hs Code.:

C<sub>24</sub>H<sub>26</sub>ClF<sub>3</sub>N<sub>4</sub>O

Synonyms:C₂₄H₂₆ClF₃N₄O

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Chemical Property of C₂₄H₂₆ClF₃N₄O

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Technology Process of C₂₄H₂₆ClF₃N₄O

There total 8 articles about C₂₄H₂₆ClF₃N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: C₂₉H₃₇ClF₃IN₄O₇

: 1037361-22-0
C₂₄H₂₆ClF₃N₄O

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2.5h;
DOI:10.1016/j.bmcl.2013.12.118

Reference yield:

: 65619-29-6
1-(3-chlorophenyl)-4-oxocyclohexanecarbonitrile

: 1037361-22-0
C₂₄H₂₆ClF₃N₄O

Guidance literature:: Multi-step reaction with 7 steps

1: toluene-4-sulfonic acid / toluene / 18 h / Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 - 50 °C

3: triethylamine / dichloromethane / 4 h / 20 °C

4: pyridinium p-toluenesulfonate / acetone; water / 48 h / Reflux

5: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane; acetic acid / 5 h / 20 °C

6: ruthenium dioxide dihydrate; sodium periodate / chloroform; acetonitrile; water / 0.33 h / 20 °C

7: hydrogenchloride / 1,4-dioxane / 2.5 h / 20 °C

With hydrogenchloride; sodium periodate; lithium aluminium tetrahydride; ruthenium dioxide dihydrate; pyridinium p-toluenesulfonate; sodium tris(acetoxy)borohydride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; chloroform; water; acetic acid; 1,2-dichloro-ethane; acetone; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2013.12.118

Reference yield:

: 887978-99-6
C-[8-(3-chlorophenyl)-1.4-dioxa-spiro[4.5]dec-8-yl]methylamine

: 1037361-22-0
C₂₄H₂₆ClF₃N₄O

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 4 h / 20 °C

2: pyridinium p-toluenesulfonate / acetone; water / 48 h / Reflux

3: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane; acetic acid / 5 h / 20 °C

4: ruthenium dioxide dihydrate; sodium periodate / chloroform; acetonitrile; water / 0.33 h / 20 °C

5: hydrogenchloride / 1,4-dioxane / 2.5 h / 20 °C

With hydrogenchloride; sodium periodate; ruthenium dioxide dihydrate; pyridinium p-toluenesulfonate; sodium tris(acetoxy)borohydride; triethylamine; In 1,4-dioxane; dichloromethane; chloroform; water; acetic acid; 1,2-dichloro-ethane; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2013.12.118