N,N'-bis(methyl 4,6-O-benzylidene-3-deoxy-α-D-altropyrano-3-yl)-1,2-diaminoethane

Base Information

Chemical Name:N,N'-bis(methyl 4,6-O-benzylidene-3-deoxy-α-D-altropyrano-3-yl)-1,2-diaminoethane
CAS No.:945035-12-1
Molecular Formula:C₃₀H₄₀N₂O₁₀
Molecular Weight:588.655
Hs Code.:

Synonyms:N,N'-bis(methyl 4,6-O-benzylidene-3-deoxy-α-D-altropyrano-3-yl)-1,2-diaminoethane

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Chemical Property of N,N'-bis(methyl 4,6-O-benzylidene-3-deoxy-α-D-altropyrano-3-yl)-1,2-diaminoethane

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Technology Process of N,N'-bis(methyl 4,6-O-benzylidene-3-deoxy-α-D-altropyrano-3-yl)-1,2-diaminoethane

There total 1 articles about N,N'-bis(methyl 4,6-O-benzylidene-3-deoxy-α-D-altropyrano-3-yl)-1,2-diaminoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 107-15-3,85404-18-8
ethylenediamine

: 3150-15-0,3150-16-1,3257-59-8,14187-71-4,15384-57-3,19465-13-5,32976-15-1,52885-37-7,53270-02-3,53270-03-4,65391-11-9,65391-12-0,66537-92-6,67226-04-4,71184-14-0,86420-78-2,86420-79-3,91177-51-4,91177-52-5,117708-93-7,120408-72-2,2880-96-8
methyl 2,3-anhydro-4,6-O-benzilidene-α-D-mannopyranoside

: 945035-12-1
N,N'-bis(methyl 4,6-O-benzylidene-3-deoxy-α-D-altropyrano-3-yl)-1,2-diaminoethane

Guidance literature:: In methanol; at 140 ℃; for 12h;
DOI:10.1002/ejic.200700027

Reference yield: 92.0%

: 945035-12-1
N,N'-bis(methyl 4,6-O-benzylidene-3-deoxy-α-D-altropyrano-3-yl)-1,2-diaminoethane

: 122-51-0
orthoformic acid triethyl ester

: N,N'-1,3-bis(methyl 4,6-O-benzylidene-3-deoxy-α-D-altropyrano-3-yl)imidazolinium chloride

Guidance literature:: With ammonium chloride; at 110 ℃; for 3h;
DOI:10.1002/ejic.200700027

Reference yield:

: 945035-12-1
N,N'-bis(methyl 4,6-O-benzylidene-3-deoxy-α-D-altropyrano-3-yl)-1,2-diaminoethane

: N,N'-1,3-bis(methyl 4,6-O-benzylidene-3-deoxy-α-D-altropyrano-3-yl)-2-hydroxyimidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NH₄Cl / 3 h / 110 °C

2: sodium tert-butoxide; [RhCl(COD)]2 / tetrahydrofuran / 48 h / 45 °C

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; ammonium chloride; sodium t-butanolate; In tetrahydrofuran;
DOI:10.1002/ejic.200700027