Methyl threo-4-<1,2-dihydroxy-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)ethyl>benzoate

Base Information

Chemical Name:Methyl threo-4-<1,2-dihydroxy-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)ethyl>benzoate
CAS No.:119436-69-0
Molecular Formula:C₂₄H₃₀O₄
Molecular Weight:382.5
Hs Code.:

Synonyms:Methyl threo-4-<1,2-dihydroxy-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)ethyl>benzoate

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Chemical Property of Methyl threo-4-<1,2-dihydroxy-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)ethyl>benzoate

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Technology Process of Methyl threo-4-<1,2-dihydroxy-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)ethyl>benzoate

There total 4 articles about Methyl threo-4-<1,2-dihydroxy-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)ethyl>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.2%

: 102121-54-0
Methyl (E)-4-<2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)ethenyl>benzoate

: 119436-69-0
Methyl threo-4-<1,2-dihydroxy-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)ethyl>benzoate

Guidance literature:: With pyridine; osmium(VIII) oxide; for 1h;
DOI:10.1021/jm00125a027

Reference yield:

: 6683-48-3
1,1,4,4,6-pentamethyl-1,2,3,4-tetrahydronaphthalene

: 119436-69-0
Methyl threo-4-<1,2-dihydroxy-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)ethyl>benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: N-bromosuccinimide, azobisisobutyronitrile / CHCl₃

2: benzene / 5 h / Heating

3: NaOMe / methanol

4: 94.2 percent / OsO₄, pyridine / 1 h

With pyridine; N-Bromosuccinimide; osmium(VIII) oxide; 2,2'-azobis(isobutyronitrile); sodium methylate; In methanol; chloroform; benzene;
DOI:10.1021/jm00125a027

Reference yield:

: 119435-90-4
(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-bromomethane

: 119436-69-0
Methyl threo-4-<1,2-dihydroxy-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)ethyl>benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 5 h / Heating

2: NaOMe / methanol

3: 94.2 percent / OsO₄, pyridine / 1 h

With pyridine; osmium(VIII) oxide; sodium methylate; In methanol; benzene;
DOI:10.1021/jm00125a027