O-triethylsilyl-2-ethanol

Base Information

Chemical Name:O-triethylsilyl-2-ethanol
CAS No.:162470-09-9
Molecular Formula:C₁₉H₂₈F₃NO₂Si
Molecular Weight:387.518
Hs Code.:

O-triethylsilyl-2-<o-(N-allyl,N-trifluoroacetylamino)phenyl>ethanol

Synonyms:O-triethylsilyl-2-ethanol

Suppliers and Price of O-triethylsilyl-2-ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-triethylsilyl-2-ethanol

Chemical Property:

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Technology Process of O-triethylsilyl-2-ethanol

There total 4 articles about O-triethylsilyl-2-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 106-95-6
allyl bromide

: 163531-19-9
O-triethylsilyl-2-ethanol

: 162470-09-9
O-triethylsilyl-2-ethanol

Guidance literature:: With potassium carbonate;
DOI:10.1016/0040-4039(94)02488-W

Reference yield:

: 994-30-9
triethylsilyl chloride

: 162470-09-9
O-triethylsilyl-2-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / Et₃N / CH₂Cl₂ / 1 h / -20 °C

2: 94 percent / Et₃N / diethyl ether / 0.5 h / -20 °C

3: 93 percent / Na₂CO₃ / acetone / Ambient temperature

With sodium carbonate; triethylamine; In diethyl ether; dichloromethane; acetone;
DOI:10.1016/0040-4020(96)00249-9

Reference yield:

: 5339-85-5
2-aminophenethyl alcohol

: 162470-09-9
O-triethylsilyl-2-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / Et₃N / CH₂Cl₂ / 1 h / -20 °C

2: 94 percent / Et₃N / diethyl ether / 0.5 h / -20 °C

3: 93 percent / Na₂CO₃ / acetone / Ambient temperature

With sodium carbonate; triethylamine; In diethyl ether; dichloromethane; acetone;
DOI:10.1016/0040-4020(96)00249-9