Technology Process of C22H22O5
There total 6 articles about C22H22O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: aluminum (III) chloride / dichloromethane / 1 h / 0 - 20 °C
2.1: sulfur; morpholine / 12 h / 130 °C
2.2: 12 h / Reflux
3.1: boron trifluoride diethyl etherate / 0.17 h / 100 °C
3.2: 0.33 h / 55 °C
3.3: 3 h / 80 °C
4.1: acetic acid; hydrogen; platinum on carbon / 12 h / 100 °C
5.1: acetic acid; phenylboronic acid / toluene / 12 h / Reflux; Inert atmosphere
With
morpholine; aluminum (III) chloride; platinum on carbon; boron trifluoride diethyl etherate; hydrogen; sulfur; acetic acid; phenylboronic acid;
In
dichloromethane; toluene;
DOI:10.1080/00397911.2013.821616
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydroxide / water / 3 h / 0 - 70 °C
2.1: aluminum (III) chloride / dichloromethane / 1 h / 0 - 20 °C
3.1: sulfur; morpholine / 12 h / 130 °C
3.2: 12 h / Reflux
4.1: boron trifluoride diethyl etherate / 0.17 h / 100 °C
4.2: 0.33 h / 55 °C
4.3: 3 h / 80 °C
5.1: acetic acid; hydrogen; platinum on carbon / 12 h / 100 °C
6.1: acetic acid; phenylboronic acid / toluene / 12 h / Reflux; Inert atmosphere
With
morpholine; aluminum (III) chloride; platinum on carbon; boron trifluoride diethyl etherate; hydrogen; sulfur; acetic acid; sodium hydroxide; phenylboronic acid;
In
dichloromethane; water; toluene;
DOI:10.1080/00397911.2013.821616
