8-imino-1,7-naphthyridin-7(8H)-amine 2,4,6-trimethylbenzenesulfonate

Base Information

Chemical Name:8-imino-1,7-naphthyridin-7(8H)-amine 2,4,6-trimethylbenzenesulfonate
CAS No.:1351516-28-3
Molecular Formula:C₈H₈N₄*C₉H₁₂O₃S
Molecular Weight:360.437
Hs Code.:

Synonyms:8-imino-1,7-naphthyridin-7(8H)-amine 2,4,6-trimethylbenzenesulfonate

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Chemical Property of 8-imino-1,7-naphthyridin-7(8H)-amine 2,4,6-trimethylbenzenesulfonate

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Technology Process of 8-imino-1,7-naphthyridin-7(8H)-amine 2,4,6-trimethylbenzenesulfonate

There total 5 articles about 8-imino-1,7-naphthyridin-7(8H)-amine 2,4,6-trimethylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 36016-40-7
mesitylenesulfonylhydroxylamine

: 17965-82-1
8-amino-1,7-naphthyridine

: 1351516-28-3
8-imino-1,7-naphthyridin-7(8H)-amine 2,4,6-trimethylbenzenesulfonate

Guidance literature:: In dichloromethane; at 0 ℃; for 2h;

Reference yield:

: 452-58-4
2,3-Diaminopyridine

: 1351516-28-3
8-imino-1,7-naphthyridin-7(8H)-amine 2,4,6-trimethylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid; sodium 3-nitrobenzenesulfonate / water / 16 h / 135 °C

1.2: pH ~ 9

2.1: dichloromethane / 2 h / 0 °C

With sulfuric acid; sodium 3-nitrobenzenesulfonate; In dichloromethane; water;

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 1351516-28-3
8-imino-1,7-naphthyridin-7(8H)-amine 2,4,6-trimethylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / diethyl ether / 20 °C

2: trifluoroacetic acid / 0.67 h / 10 °C

3: dichloromethane / 2 h / 0 °C

With triethylamine; trifluoroacetic acid; In diethyl ether; dichloromethane;