ethyl 2-[1-[(4-methylthio)phenyl]-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate

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Chemical Name:ethyl 2-[1-[(4-methylthio)phenyl]-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate
CAS No.:1346223-06-0
Molecular Formula:C₂₃H₂₅NO₄S₂
Molecular Weight:443.588
Hs Code.:

Synonyms:ethyl 2-[1-[(4-methylthio)phenyl]-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate

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Chemical Property of ethyl 2-[1-[(4-methylthio)phenyl]-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate

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Technology Process of ethyl 2-[1-[(4-methylthio)phenyl]-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate

There total 5 articles about ethyl 2-[1-[(4-methylthio)phenyl]-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1346223-05-9
ethyl 2-[1-(4-methylthiophenyl)-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]glyoxylate

: 1346223-06-0
ethyl 2-[1-[(4-methylthio)phenyl]-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate

Guidance literature:: With triethylsilane; trifluoroacetic acid;

Reference yield:

: 189501-33-5
1-[4-(methylthio)phenyl]pentane-1,4-dione

: 1346223-06-0
ethyl 2-[1-[(4-methylthio)phenyl]-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium peroxomonosulfate / methanol; water / 20 °C

2: toluene-4-sulfonic acid / ethanol / 0.75 h / 160 °C / 7757.43 Torr / Microwave irradiation

3: titanium tetrachloride / dichloromethane / 0 - 20 °C / Inert atmosphere

4: triethylsilane; trifluoroacetic acid / 0 - 20 °C / Inert atmosphere

With triethylsilane; potassium peroxomonosulfate; titanium tetrachloride; toluene-4-sulfonic acid; trifluoroacetic acid; In methanol; ethanol; dichloromethane; water;
DOI:10.1021/jm200715n

Reference yield:

: 1-[(4-methylthio)phenyl]-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrole

: 1346223-06-0
ethyl 2-[1-[(4-methylthio)phenyl]-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-pyrrol-3-yl]acetate

Guidance literature:: Multi-step reaction with 2 steps

1: titanium tetrachloride / dichloromethane / 0 - 20 °C / Inert atmosphere

2: triethylsilane; trifluoroacetic acid / 0 - 20 °C / Inert atmosphere

With triethylsilane; titanium tetrachloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm200715n