ethyl 2-methyl-2-[4-(2-{4-[(2E)-3-phenylprop-2-enoyl]phenoxy}ethyl)phenoxy]propanoate

Base Information

• Chemical Name: ethyl 2-methyl-2-[4-(2-{4-[(2E)-3-phenylprop-2-enoyl]phenoxy}ethyl)phenoxy]propanoate
• CAS No.: 1415608-82-0
• Molecular Formula: C₂₉H₃₀O₅
• Molecular Weight: 458.554

Synonyms:ethyl 2-methyl-2-[4-(2-{4-[(2E)-3-phenylprop-2-enoyl]phenoxy}ethyl)phenoxy]propanoate

Chemical Property of ethyl 2-methyl-2-[4-(2-{4-[(2E)-3-phenylprop-2-enoyl]phenoxy}ethyl)phenoxy]propanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 2-methyl-2-[4-(2-{4-[(2E)-3-phenylprop-2-enoyl]phenoxy}ethyl)phenoxy]propanoate

There total 3 articles about ethyl 2-methyl-2-[4-(2-{4-[(2E)-3-phenylprop-2-enoyl]phenoxy}ethyl)phenoxy]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

ethyl 2-[4-(2-hydroxyethyl)phenoxy]-2-methylpropanoate (167213-41-4) + (E)-1-(4-hydroxyphenyl)-3-phenylprop-2-en-1-one (2657-25-2) → ethyl 2-methyl-2-[4-(2-{4-[(2E)-3-phenylprop-2-enoyl]phenoxy}ethyl)phenoxy]propanoate (1415608-82-0)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.bmcl.2012.09.111

Reference yield:

ethyl 2-bromoisobutyrate (600-00-0) → ethyl 2-methyl-2-[4-(2-{4-[(2E)-3-phenylprop-2-enoyl]phenoxy}ethyl)phenoxy]propanoate (1415608-82-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / Reflux

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2012.09.111

Reference yield:

p-hydroxyphenethyl alcohol (501-94-0) → ethyl 2-methyl-2-[4-(2-{4-[(2E)-3-phenylprop-2-enoyl]phenoxy}ethyl)phenoxy]propanoate (1415608-82-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / Reflux

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2012.09.111

upstream raw materials:

ethyl 2-bromoisobutyrate

ethyl 2-[4-(2-hydroxyethyl)phenoxy]-2-methylpropanoate

(E)-1-(4-hydroxyphenyl)-3-phenylprop-2-en-1-one

p-hydroxyphenethyl alcohol

Downstream raw materials:

C₂₇H₂₆O₅

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1415608-82-0 ethyl 2-methyl-2-[4-(2-{4-[(2E)-3-phenylprop-2-enoyl]phenoxy}ethyl)phenoxy]propanoate

Send

Send

Metric Ton KG G Pound L ML

Send

Send