(-)-2-(benzyloxy)-3-hydroxypropyl benzoate

Base Information Edit

Chemical Name:(-)-2-(benzyloxy)-3-hydroxypropyl benzoate
CAS No.:109430-97-9
Molecular Formula:C₁₇H₁₈O₄
Molecular Weight:286.328
Hs Code.:
Mol file:109430-97-9.mol

Synonyms:(-)-2-(benzyloxy)-3-hydroxypropyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-2-(benzyloxy)-3-hydroxypropyl benzoate Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of (-)-2-(benzyloxy)-3-hydroxypropyl benzoate

There total 8 articles about (-)-2-(benzyloxy)-3-hydroxypropyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 109371-34-8
Benzoic acid (S)-3-acetoxy-2-benzyloxy-propyl ester

: 109430-97-9
(-)-2-(benzyloxy)-3-hydroxypropyl benzoate

Guidance literature:: In di-isopropyl ether; water; Ambient temperature; pH 7, Lipase aus Schweinepankreas, Fluka;
DOI:10.1016/S0040-4039(00)95774-5

Reference yield:

: 145484-35-1
Benzoic acid (R)-2-benzyloxy-3-oxo-propyl ester

: 109430-97-9
(-)-2-(benzyloxy)-3-hydroxypropyl benzoate

Guidance literature:: With sodium cyanoborohydride; In methanol; acetic acid; for 1h; Yield given; Ambient temperature;
DOI:10.1246/bcsj.65.2643

Reference yield:

: 17618-04-1
2,5-di-O-benzyl-D-mannitol

: 109430-97-9
(-)-2-(benzyloxy)-3-hydroxypropyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 92.8 percent / pyridine / 6 h / -18 °C

2: HIO₄*2H₂O / ethanol / 1 h / Ambient temperature

3: NaBH₃CN / methanol; acetic acid / 1 h / Ambient temperature

With pyridine; sodium cyanoborohydride; periodic acid; In methanol; ethanol; acetic acid;
DOI:10.1246/bcsj.65.2643