(ethylene)bis(triethylphosphine)platinum⁽⁰⁾

Base Information

Chemical Name:(ethylene)bis(triethylphosphine)platinum⁽⁰⁾
CAS No.:76136-93-1
Molecular Formula:C₁₄H₃₄P₂Pt
Molecular Weight:459.451
Hs Code.:

(ethylene)bis(triethylphosphine)platinum<sup>(0)</sup>

Synonyms:(ethylene)bis(triethylphosphine)platinum⁽⁰⁾

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Chemical Property of (ethylene)bis(triethylphosphine)platinum⁽⁰⁾

Chemical Property:

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Technology Process of (ethylene)bis(triethylphosphine)platinum⁽⁰⁾

There total 2 articles about (ethylene)bis(triethylphosphine)platinum⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75847-39-1,76189-28-1
diethylbis(triethylphosphine)platinum(II)

: 76136-93-1
(ethylene)bis(triethylphosphine)platinum⁽⁰⁾

: 74-85-1
ethene

Guidance literature:: In cyclohexane; Pt-complex evacuated to 0.1 torr, flushed with Ar, dry degassed cyclohexane added, cooled (liq. N2), evacuated (0.1 torr), sealed, warmed to room temp., heated at 118°C (oil bath) for 30 min;
DOI:10.1021/ic50218a073

Reference yield:

: 74-85-1
ethene

: 1352241-85-0
cis-[Pt(H)(Si(OEt)3)(PEt₃)2]

: 1352241-85-0
trans-[Pt(H)(Si(OEt)3)(PEt₃)2]

: 76136-93-1
(ethylene)bis(triethylphosphine)platinum⁽⁰⁾

: 201860-25-5
cis-Pt(PEt₃)2(H)(SiPh₃)

Guidance literature:: In benzene-d6; acetonitrile; byproducts: HSi(OCH2CH3)3; Schlenk technique or glovebox; ethene bubbled into soln. of Pt-complexesin MeCN/C6D6 at room temp. for 10 min, soln. stored at room temp. for 5 d; detected by NMR spectroscopy and MS;
DOI:10.1039/c1dt11351h

Reference yield:

: 82265-68-7
(1,2,3-triphenylphosphirene)pentacarbonyltungsten

: 76136-93-1
(ethylene)bis(triethylphosphine)platinum⁽⁰⁾

: PtW(CO)5(P(C₂H₅)3)2(C₆H₅PC₂(C₆H₅)2)

Guidance literature:: In not given; W complex was treated with Pt complex (generated in situ by treating PtH2(PEt3)2 with ethylene) under mild conditions; satisfactory elem. anal.;
DOI:10.1039/c39860000762