methyl 4-<4-prop-2-ynylamino>phenyl>butyrate

Base Information

Chemical Name:methyl 4-<4-prop-2-ynylamino>phenyl>butyrate
CAS No.:101248-44-6
Molecular Formula:C₂₃H₂₄N₄O₃
Molecular Weight:404.469
Hs Code.:

methyl 4-<4-<N-<(2-amino-4-hydroxy-6-quinazolinyl)methyl>prop-2-ynylamino>phenyl>butyrate

Synonyms:methyl 4-<4-prop-2-ynylamino>phenyl>butyrate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-<4-prop-2-ynylamino>phenyl>butyrate

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Technology Process of methyl 4-<4-prop-2-ynylamino>phenyl>butyrate

There total 2 articles about methyl 4-<4-prop-2-ynylamino>phenyl>butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.8%

: 77766-62-2
2-amino-6-(bromomethyl)-4-hydroxyquinazoline hydrobromide

: 101248-43-5
methyl 4-<4-(prop-2-ynylamino)phenyl>butyrate

: 101248-44-6
methyl 4-<4-prop-2-ynylamino>phenyl>butyrate

Guidance literature:: With calcium carbonate; In various solvent(s); at 25 ℃; for 25.5h;
DOI:10.1021/jm00156a033

Reference yield:

: 20637-09-6
methyl 4-(4-aminophenyl)butanoate

: 101248-44-6
methyl 4-<4-prop-2-ynylamino>phenyl>butyrate

Guidance literature:: Multi-step reaction with 2 steps

1: 26 percent / K₂CO₃ / methanol / 3 h / Heating

2: 29.8 percent / CaCO₃ / various solvent(s) / 25.5 h / 25 °C

With potassium carbonate; calcium carbonate; In methanol;
DOI:10.1021/jm00156a033