C₁₈H₁₈Cl₂N₂O₅S

Base Information

Chemical Name:C₁₈H₁₈Cl₂N₂O₅S
CAS No.:1408186-96-8
Molecular Formula:C₁₈H₁₈Cl₂N₂O₅S
Molecular Weight:445.323
Hs Code.:

C<sub>18</sub>H<sub>18</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>5</sub>S

Synonyms:C₁₈H₁₈Cl₂N₂O₅S

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Chemical Property of C₁₈H₁₈Cl₂N₂O₅S

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Technology Process of C₁₈H₁₈Cl₂N₂O₅S

There total 6 articles about C₁₈H₁₈Cl₂N₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 1408186-92-4
ethyl (2R,3S)-3-(benzyloxy)-1-((3,4-dichlorophenyl)sulfonyl)pyrrolidine-2-carboxylate

: 1408186-96-8
C₁₈H₁₈Cl₂N₂O₅S

Guidance literature:: With hydroxylamine hydrochloride; potassium hydroxide; In methanol; at 80 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.08.028

Reference yield:

: 170123-25-8
3-oxo-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester 2-ethyl ester

: 1408186-96-8
C₁₈H₁₈Cl₂N₂O₅S

Guidance literature:: Multi-step reaction with 5 steps

1: calcium chloride; Sucrose / water / 48 h / 30 °C / Microbiological reaction

2: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

4: triethylamine; dmap / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

5: hydroxylamine hydrochloride; potassium hydroxide / methanol / 1 h / 80 °C / Inert atmosphere

With dmap; hydroxylamine hydrochloride; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; trifluoroacetic acid; calcium chloride; potassium hydroxide; Sucrose; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.ejmech.2012.08.028

Reference yield:

: 3783-61-7
diethyl 2-azabutane-1,4-dicarboxylate

: 1408186-96-8
C₁₈H₁₈Cl₂N₂O₅S

Guidance literature:: Multi-step reaction with 7 steps

1: sodium hydroxide / chloroform; water / 73 h / 0 - 20 °C

2: potassium tert-butylate / toluene / 1.5 h / -10 - 0 °C / Inert atmosphere

3: calcium chloride; Sucrose / water / 48 h / 30 °C / Microbiological reaction

4: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

5: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

6: triethylamine; dmap / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

7: hydroxylamine hydrochloride; potassium hydroxide / methanol / 1 h / 80 °C / Inert atmosphere

With dmap; hydroxylamine hydrochloride; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; trifluoroacetic acid; calcium chloride; potassium hydroxide; sodium hydroxide; Sucrose; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; toluene;
DOI:10.1016/j.ejmech.2012.08.028