(+/-)-3-(2-(4-benzyl-4-(dimethylamino)cyclohex-1-enyl)-1H-indol-3-yl)propan-1-ol, citrate

Base Information

Chemical Name:(+/-)-3-(2-(4-benzyl-4-(dimethylamino)cyclohex-1-enyl)-1H-indol-3-yl)propan-1-ol, citrate
CAS No.:1004541-99-4
Molecular Formula:C₆H₈O₇*C₂₆H₃₂N₂O
Molecular Weight:580.678
Hs Code.:

Synonyms:(+/-)-3-(2-(4-benzyl-4-(dimethylamino)cyclohex-1-enyl)-1H-indol-3-yl)propan-1-ol, citrate

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Chemical Property of (+/-)-3-(2-(4-benzyl-4-(dimethylamino)cyclohex-1-enyl)-1H-indol-3-yl)propan-1-ol, citrate

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Technology Process of (+/-)-3-(2-(4-benzyl-4-(dimethylamino)cyclohex-1-enyl)-1H-indol-3-yl)propan-1-ol, citrate

There total 2 articles about (+/-)-3-(2-(4-benzyl-4-(dimethylamino)cyclohex-1-enyl)-1H-indol-3-yl)propan-1-ol, citrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1004541-98-3
(+/-)-3-(2-(4-Benzyl-4-(dimethylamino)cyclohex-1-enyl)-1H-indol-3-yl)propan-1-ol

: 77-92-9,906507-37-7
citric acid

: 1004541-99-4
(+/-)-3-(2-(4-benzyl-4-(dimethylamino)cyclohex-1-enyl)-1H-indol-3-yl)propan-1-ol, citrate

Guidance literature:: In isopropyl alcohol; at 5 ℃;

Reference yield:

: 475098-34-1
4-benzyl-4-(dimethylamino)cyclohexanone

: 1004547-88-9
3-(3-trimethylsilanyloxypropyl)-1H-indole

: 1004541-99-4
(+/-)-3-(2-(4-benzyl-4-(dimethylamino)cyclohex-1-enyl)-1H-indol-3-yl)propan-1-ol, citrate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluorormethanesulfonic acid / dichloromethane / 24 h / 20 °C

1.2: 0.33 h / 20 °C

2.1: isopropyl alcohol / 5 °C

With trifluorormethanesulfonic acid; In dichloromethane; isopropyl alcohol;