N¹-(N²,N⁶-bis(2,3-dibenzyloxybenzoyl)-L-lysyl)-N⁴-(2,3-dibenzyloxybenzoyl)-1,4-diaminobutane

Base Information

• Chemical Name: N¹-(N²,N⁶-bis(2,3-dibenzyloxybenzoyl)-L-lysyl)-N⁴-(2,3-dibenzyloxybenzoyl)-1,4-diaminobutane
• CAS No.: 173062-74-3
• Molecular Formula: C₇₃H₇₂N₄O₁₀
• Molecular Weight: 1165.4

Synonyms:N¹-(N²,N⁶-bis(2,3-dibenzyloxybenzoyl)-L-lysyl)-N⁴-(2,3-dibenzyloxybenzoyl)-1,4-diaminobutane

Chemical Property of N¹-(N²,N⁶-bis(2,3-dibenzyloxybenzoyl)-L-lysyl)-N⁴-(2,3-dibenzyloxybenzoyl)-1,4-diaminobutane

Chemical Property:

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Technology Process of N¹-(N²,N⁶-bis(2,3-dibenzyloxybenzoyl)-L-lysyl)-N⁴-(2,3-dibenzyloxybenzoyl)-1,4-diaminobutane

There total 2 articles about N¹-(N²,N⁶-bis(2,3-dibenzyloxybenzoyl)-L-lysyl)-N⁴-(2,3-dibenzyloxybenzoyl)-1,4-diaminobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

(S)-2,6-bis[(2,3-dibenzyloxybenzoyl)amino]hexanoic acid (96920-78-4) + N-(aminobutyl)-2,3-bis(benzyloxy)benzamide (192802-99-6) → N1-(N2,N6-bis(2,3-dibenzyloxybenzoyl)-L-lysyl)-N4-(2,3-dibenzyloxybenzoyl)-1,4-diaminobutane (173062-74-3)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile; for 5h; Ambient temperature;

Reference yield:

2,3-dibenzyloxybenzoic acid (74272-78-9) → N1-(N2,N6-bis(2,3-dibenzyloxybenzoyl)-L-lysyl)-N4-(2,3-dibenzyloxybenzoyl)-1,4-diaminobutane (173062-74-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) N,N'-carbonyldiimidazole / 1) THF, 2) THF, r.t., overnight

2: 84 percent / iPr₂NEt, 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate / tetrahydrofuran; acetonitrile / 5 h / Ambient temperature

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; acetonitrile;

Reference yield: 98.0%

N1-(N2,N6-bis(2,3-dibenzyloxybenzoyl)-L-lysyl)-N4-(2,3-dibenzyloxybenzoyl)-1,4-diaminobutane (173062-74-3) → 1-N-[2-N',6-N''-bis(2,3-dihydroxybenzoyl)-L-lysyl]-4-N-(2,3-dihydroxybenzoyl)-1,4-diaminobutane (131610-88-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; benzene; Ambient temperature;

upstream raw materials:

(S)-2,6-bis[(2,3-dibenzyloxybenzoyl)amino]hexanoic acid

N-(aminobutyl)-2,3-bis(benzyloxy)benzamide

2,3-dibenzyloxybenzoic acid

Downstream raw materials:

1-N-[2-N',6-N''-bis(2,3-dihydroxybenzoyl)-L-lysyl]-4-N-(2,3-dihydroxybenzoyl)-1,4-diaminobutane

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