2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(3',5'-di-O-t-butyldimethylsilyl-2'-deoxy-β-D-ribofuranosyl)purine

Base Information

Chemical Name:2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(3',5'-di-O-t-butyldimethylsilyl-2'-deoxy-β-D-ribofuranosyl)purine
CAS No.:1204045-48-6
Molecular Formula:C₄₃H₆₉N₅O₆Si₂
Molecular Weight:808.222
Hs Code.:

Synonyms:2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(3',5'-di-O-t-butyldimethylsilyl-2'-deoxy-β-D-ribofuranosyl)purine

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Chemical Property of 2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(3',5'-di-O-t-butyldimethylsilyl-2'-deoxy-β-D-ribofuranosyl)purine

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Technology Process of 2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(3',5'-di-O-t-butyldimethylsilyl-2'-deoxy-β-D-ribofuranosyl)purine

There total 2 articles about 2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(3',5'-di-O-t-butyldimethylsilyl-2'-deoxy-β-D-ribofuranosyl)purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1204045-49-7
3-tri(n-butyl)tin-2-propenyl menthyl ether

: 1204045-46-4
2-N-phenoxyacetyl-6-O-p-toluenesulphonyl-3',5'-di-O-t-butyldimethylsilyl-2'-deoxyguanosine

: 1204045-48-6
2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(3',5'-di-O-t-butyldimethylsilyl-2'-deoxy-β-D-ribofuranosyl)purine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride; In 1,4-dioxane; at 110 ℃; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2009.10.023

Reference yield: 22.0%

: 1204045-47-5
2-N-phenoxyacetyl-6-vinyl-3',5'-di-O-t-butyldimethylsilyl-2'-deoxyguanosine

: 40940-58-7,144266-44-4,67528-21-6
(1S,2R,4R)-2-(allyloxy)-1-isopropyl-4-methylcyclohexane

: 1204045-48-6
2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(3',5'-di-O-t-butyldimethylsilyl-2'-deoxy-β-D-ribofuranosyl)purine

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 45 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.10.023

Reference yield: 95.0%

: 1204045-48-6
2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(3',5'-di-O-t-butyldimethylsilyl-2'-deoxy-β-D-ribofuranosyl)purine

: 1204045-50-0
2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(2'-deoxy-β-D-ribofuranosyl)purine

Guidance literature:: 2-N-phenoxyacetyl-6-(3-O-L-menthylpropenyl)-9-(3',5'-di-O-t-butyldimethylsilyl-2'-deoxy-β-D-ribofuranosyl)purine; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With methanol; In dichloromethane;
DOI:10.1016/j.tet.2009.10.023