allyl menthyl ether

Base Information

• Chemical Name: allyl menthyl ether
• CAS No.: 40940-58-7
• Molecular Formula: C₁₃H₂₄O
• Molecular Weight: 196.333
• Mol file: 40940-58-7.mol

Synonyms:

Chemical Property of allyl menthyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of allyl menthyl ether

There total 12 articles about allyl menthyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(-)-menthol (2216-51-5) + allyl bromide (106-95-6) → (1S,2R,4R)-2-(allyloxy)-1-isopropyl-4-methylcyclohexane (40940-58-7,144266-44-4,67528-21-6)

Guidance literature:

With 1H-imidazole; tetra-(n-butyl)ammonium iodide; sodium hydride;

DOI:10.1016/0040-4039(96)01540-7

Reference yield: 92.0%

(-)-menthol (2216-51-5) + triallyl cyanurate (101-37-1,25988-85-6) → (1S,2R,4R)-2-(allyloxy)-1-isopropyl-4-methylcyclohexane (40940-58-7,144266-44-4,67528-21-6)

Guidance literature:

With trifluorormethanesulfonic acid; In 1,4-dioxane; at 50 ℃; for 5.5h; Temperature; Catalytic behavior; Molecular sieve;

DOI:10.1248/cpb.c16-00744

Reference yield: 83.8%

(-)-menthol (2216-51-5) → (1S,2R,4R)-2-(allyloxy)-1-isopropyl-4-methylcyclohexane (40940-58-7,144266-44-4,67528-21-6)

Guidance literature:

(-)-menthol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h;

All-X; In tetrahydrofuran; at 0 ℃;

DOI:10.1021/ol049135q

upstream raw materials:

sodium menthoxide

allyl bromide

(-)-menthol

allyl iodid

Downstream raw materials:

((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-[3-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-propyl]-dimethyl-silane

Chloro-[3-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-propyl]-dimethyl-silane

(-)-menthol

(1S,2R,4R)-1-isopropyl-4-methyl-2-((Z)-prop-1-en-1-yloxy)cyclohexane