benzyl 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside

Base Information

Chemical Name:benzyl 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside
CAS No.:77886-96-5
Molecular Formula:C₃₉H₄₀O₁₆
Molecular Weight:764.737
Hs Code.:

benzyl 5-O<methyl (2',3',4'-tri-O-acetyl-β-D-glucopyranosyl)uronate>-2,3-di-O-benzoyl-β-D-ribofuranoside

Synonyms:benzyl 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside

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Technology Process of benzyl 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside

There total 1 articles about benzyl 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.6%

: 77886-95-4
C₂₆H₂₄O₇

: 21085-72-3
1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester

: 77886-96-5
benzyl 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside

Guidance literature:: With mercury(II) cyanide; In nitromethane; dichloromethane; benzene; for 4h; Heating;
DOI:10.1021/jm00139a026

Reference yield:

: 77886-96-5
benzyl 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside

: 2',3'-di-O-benzoyl-5'-O-(methyl 2'',3'',4''-tri-O-acetyl-β-D-glucopyranosyluronate)-5-fluorocytidine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / H₂ / 10percent Pd/C / acetic acid; H₂O / 120 h / 2128 Torr

2: 1.) PPh₃ / 1.) MeCN, CCl₄, reflux, 3 h, 2.) MeCN, reflux, 24 h

With hydrogen; triphenylphosphine; palladium on activated charcoal; In water; acetic acid;
DOI:10.1021/jm00139a026