1-(4-(chloromethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane

Base Information

• Chemical Name: 1-(4-(chloromethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane
• CAS No.: 1163733-05-8
• Molecular Formula: C₁₇H₂₇ClO₅
• Molecular Weight: 346.851
• Mol file: 1163733-05-8.mol

Synonyms:1-(4-(chloromethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane

Chemical Property of 1-(4-(chloromethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4-(chloromethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane

There total 1 articles about 1-(4-(chloromethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

tetraethylene glycol monomethyl ether (23783-42-8,95507-80-5) + p-Xylylene dichloride (623-25-6) → 1-(4-(chloromethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane (1163733-05-8)

Guidance literature:

tetraethylene glycol monomethyl ether; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

p-Xylylene dichloride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1039/c0cc05376g

Reference yield: 90.0%

1-(4-(chloromethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane (1163733-05-8) → 1-(4-(azidomethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane (1163733-06-9)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 110 ℃; Inert atmosphere;

DOI:10.1039/c0cc05376g

Reference yield:

1-(4-(chloromethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane (1163733-05-8) → C60H90N10O15 (1163732-91-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

2: 2,6-dimethylpyridine; tetrakis(acetonitrile)copper(I) hexafluorophosphate / acetonitrile / 72 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium azide; tetrakis(acetonitrile)copper(I) hexafluorophosphate; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1039/c0cc05376g

upstream raw materials:

tetraethylene glycol monomethyl ether

p-Xylylene dichloride

Downstream raw materials:

1-(4-(azidomethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane

C₆₀H₉₀N₁₀O₁₅