trans-3-deuterio phenyl vinyl ketone

Base Information

Chemical Name:trans-3-deuterio phenyl vinyl ketone
CAS No.:64559-96-2
Molecular Formula:C₉H₈O
Molecular Weight:133.154
Hs Code.:

Synonyms:trans-3-deuterio phenyl vinyl ketone

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Chemical Property of trans-3-deuterio phenyl vinyl ketone

Chemical Property:

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Technology Process of trans-3-deuterio phenyl vinyl ketone

There total 5 articles about trans-3-deuterio phenyl vinyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64559-91-7
3-deuterio-1-phenyl-2-propane-1-ol

: 64559-96-2
trans-3-deuterio phenyl vinyl ketone

: cis-3-deuterio phenyl vinyl ketone

Guidance literature:: With chromium(VI) oxide; tert.-butylhydroperoxide; In dichloromethane; at 20 ℃; for 2h; Title compound not separated from byproducts;
DOI:10.1021/ja048251l

Reference yield:

: cis-3-deuterio phenyl vinyl ketone

: 64559-96-2
trans-3-deuterio phenyl vinyl ketone

Guidance literature:: With poly-(L)-leucine; urea-hydrogen peroxide; 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1039/b404389h

Reference yield:

: 4187-87-5
1-Phenyl-2-propyn-1-ol

: 64559-96-2
(E/Z)-3-[⁽²⁾H₁]-phenylprop-2-enone

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiAlH₄ / tetrahydrofuran

1.2: D₂O / tetrahydrofuran

2.1: Dess-Martin periodinane

With lithium aluminium tetrahydride; Dess-Martin periodane; In tetrahydrofuran;
DOI:10.1039/b404389h