N-[4-(phenylsulfonyl)buta-2,3-dienyl]-N-[3-(trimethylsilyl)propyn-2-yl]-(4-methylbenzene)sulfonamide

Base Information

Chemical Name:N-[4-(phenylsulfonyl)buta-2,3-dienyl]-N-[3-(trimethylsilyl)propyn-2-yl]-(4-methylbenzene)sulfonamide
CAS No.:943734-06-3
Molecular Formula:C₂₃H₂₇NO₄S₂Si
Molecular Weight:473.689
Hs Code.:

Synonyms:N-[4-(phenylsulfonyl)buta-2,3-dienyl]-N-[3-(trimethylsilyl)propyn-2-yl]-(4-methylbenzene)sulfonamide

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Chemical Property of N-[4-(phenylsulfonyl)buta-2,3-dienyl]-N-[3-(trimethylsilyl)propyn-2-yl]-(4-methylbenzene)sulfonamide

Chemical Property:

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Technology Process of N-[4-(phenylsulfonyl)buta-2,3-dienyl]-N-[3-(trimethylsilyl)propyn-2-yl]-(4-methylbenzene)sulfonamide

There total 5 articles about N-[4-(phenylsulfonyl)buta-2,3-dienyl]-N-[3-(trimethylsilyl)propyn-2-yl]-(4-methylbenzene)sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₇NS₂SiO₃

: 943734-06-3
N-[4-(phenylsulfonyl)buta-2,3-dienyl]-N-[3-(trimethylsilyl)propyn-2-yl]-(4-methylbenzene)sulfonamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃;
DOI:10.1016/j.tet.2007.04.005

Reference yield:

: C₂₂H₃₁NSO₄Si

: 943734-06-3
N-[4-(phenylsulfonyl)buta-2,3-dienyl]-N-[3-(trimethylsilyl)propyn-2-yl]-(4-methylbenzene)sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 146 mg / p-TsOH / methanol / 20 °C

2: triethylamine / tetrahydrofuran / -78 °C

3: m-chloroperbenzoic acid / CH₂Cl₂ / 0 °C

With toluene-4-sulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tet.2007.04.005

Reference yield:

: 943734-04-1
N-(2-hydroxy-3-butynyl)-N-[3-(trimethylsilyl)-2-propynyl]-(4-methylbenzene)sulfonamide

: 943734-06-3
N-[4-(phenylsulfonyl)buta-2,3-dienyl]-N-[3-(trimethylsilyl)propyn-2-yl]-(4-methylbenzene)sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / -78 °C

2: m-chloroperbenzoic acid / CH₂Cl₂ / 0 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2007.04.005