N-(4-bromophenyl)-N'-octyl-naphthalene-1,4,5,8-tetracarboxylic acid bisimide

Base Information

Chemical Name:N-(4-bromophenyl)-N'-octyl-naphthalene-1,4,5,8-tetracarboxylic acid bisimide
CAS No.:1290613-35-2
Molecular Formula:C₂₈H₂₅BrN₂O₄
Molecular Weight:533.422
Hs Code.:

Synonyms:N-(4-bromophenyl)-N'-octyl-naphthalene-1,4,5,8-tetracarboxylic acid bisimide

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Chemical Property of N-(4-bromophenyl)-N'-octyl-naphthalene-1,4,5,8-tetracarboxylic acid bisimide

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Technology Process of N-(4-bromophenyl)-N'-octyl-naphthalene-1,4,5,8-tetracarboxylic acid bisimide

There total 2 articles about N-(4-bromophenyl)-N'-octyl-naphthalene-1,4,5,8-tetracarboxylic acid bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.9%

: 106-40-1
4-bromo-aniline

: 203915-43-9
7-octyl-1H-isochromeno[6,5,4-def]isoquinoline-1,3,6,8(7H)-tetraone

: 1290613-35-2
N-(4-bromophenyl)-N'-octyl-naphthalene-1,4,5,8-tetracarboxylic acid bisimide

Guidance literature:: In N,N-dimethyl-formamide; at 130 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2011.12.007

Reference yield:

: 111-86-4
n-Octylamine

: 1290613-35-2
N-(4-bromophenyl)-N'-octyl-naphthalene-1,4,5,8-tetracarboxylic acid bisimide

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 15 h / Reflux; Inert atmosphere

2: N,N-dimethyl-formamide / 12 h / 130 °C / Inert atmosphere

In N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.12.007

Reference yield:

: 1290613-35-2
N-(4-bromophenyl)-N'-octyl-naphthalene-1,4,5,8-tetracarboxylic acid bisimide

: 1356245-58-3
C₆₈H₅₄N₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,3-dioxane / 12 h / 80 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / water; N,N-dimethyl-formamide / 20 h / 120 °C / Vacuum

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; caesium carbonate; In 1,3-dioxane; water; N,N-dimethyl-formamide; 2: Suzuki coupling;
DOI:10.1016/j.tet.2011.12.007