3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-glucofuranose

Base Information

Chemical Name:3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-glucofuranose
CAS No.:180404-53-9
Molecular Formula:C₁₉H₂₆N₂O₅S
Molecular Weight:394.492
Hs Code.:

Synonyms:3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-glucofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-glucofuranose

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Technology Process of 3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-glucofuranose

There total 1 articles about 3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-glucofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 103-72-0
phenyl isothiocyanate

: 16848-19-4,24384-84-7,71165-01-0,71187-80-9,73881-34-2,91067-83-3
3-amino-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 180404-53-9
3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-glucofuranose

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/0008-6215(96)00039-0

Reference yield: 83.0%

: 180404-53-9
3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-glucofuranose

: 218915-29-8
3-amino-3-deoxy-N-phenyl-β-D-glucofuranosylamine 1,3-(cyclic thiourea)

Guidance literature:: With sulfuric acid; In 1,4-dioxane; for 5h; Heating;
DOI:10.1016/S0040-4020(98)00872-2

Reference yield:

: 180404-53-9
3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-glucofuranose

: (4R,5R,6S)-4,5-dihydroxy-3-phenyl-6-(D-erythro-triitol-1'-yl)-hexahydropyrimidine-2-thione

: (4S,5R,6S)-4,5-dihydroxy-3-phenyl-6-(D-erythro-triitol-1'-yl)-hexahydropyrimidine-2-thione

Guidance literature:: With IR-45 (OH(-)) ion exchange resin; trifluoroacetic acid; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) r.t., 2.) H₂O, MeOH;