tert-butyl 3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-ylcarbamate

Base Information

Chemical Name:tert-butyl 3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-ylcarbamate
CAS No.:1315321-73-3
Molecular Formula:C₂₀H₂₂ClNO₃S
Molecular Weight:391.919
Hs Code.:

Synonyms:tert-butyl 3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-ylcarbamate

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Chemical Property of tert-butyl 3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-ylcarbamate

Chemical Property:

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Technology Process of tert-butyl 3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-ylcarbamate

There total 1 articles about tert-butyl 3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 40312-34-3
(2-Amino-4,5,6,7-tetrahydrobenzo[b]thiophen-3-yl)(4-chlorophenyl)methanone

: 1315321-73-3
tert-butyl 3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-ylcarbamate

Guidance literature:: di-tert-butyl dicarbonate; (2-Amino-4,5,6,7-tetrahydrobenzo[b]thiophen-3-yl)(4-chlorophenyl)methanone; With dmap; In 1,4-dioxane; at 40 ℃; for 16h;

With hydrazine hydrate; In 1,4-dioxane; at 20 - 40 ℃;
DOI:10.1039/c0ob01156h

Reference yield:

: 1315321-73-3
tert-butyl 3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-ylcarbamate

: 100-39-0
benzyl bromide

: C₂₇H₂₈ClNO₃S

Guidance literature:: With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1039/c0ob01156h

Reference yield:

: 1315321-73-3
tert-butyl 3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-ylcarbamate

: 77-78-1
dimethyl sulfate

: C₂₁H₂₄ClNO₃S

Guidance literature:: With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1039/c0ob01156h