C₁₈H₂₈O₅

Base Information

Chemical Name:C₁₈H₂₈O₅
CAS No.:1609268-84-9
Molecular Formula:C₁₈H₂₈O₅
Molecular Weight:324.417
Hs Code.:

C<sub>18</sub>H<sub>28</sub>O<sub>5</sub>

Synonyms:C₁₈H₂₈O₅

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Chemical Property of C₁₈H₂₈O₅

Chemical Property:

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Technology Process of C₁₈H₂₈O₅

There total 6 articles about C₁₈H₂₈O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: C₁₈H₂₆O₅

: 1609268-84-9
C₁₈H₂₈O₅

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃; for 1h; stereoselective reaction; Inert atmosphere;
DOI:10.3987/COM-13-12905

Reference yield:

: 870091-89-7
(-)-(R)-4-benzyl-3-[(2R,3S)-5-(benzyloxy)-3-hydroxy-2-methylpentanoyl]-1,3-oxazolidin-2-one

: 1609268-84-9
C₁₈H₂₈O₅

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 34 h / Inert atmosphere

2: lithium borohydride / diethyl ether; water / 1.16 h / 0 - 20 °C / Inert atmosphere

3: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 4.5 h / 20 °C / Inert atmosphere

4: benzene / 6.5 h / 80 °C / Inert atmosphere

5: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With dmap; lithium borohydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; water; benzene; 4: |Wittig Olefination;
DOI:10.3987/COM-13-12905

Reference yield:

: 1609268-81-6
C₂₅H₃₁NO₆

: 1609268-84-9
C₁₈H₂₈O₅

Guidance literature:: Multi-step reaction with 4 steps

1: lithium borohydride / diethyl ether; water / 1.16 h / 0 - 20 °C / Inert atmosphere

2: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 4.5 h / 20 °C / Inert atmosphere

3: benzene / 6.5 h / 80 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With lithium borohydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; diethyl ether; dichloromethane; water; benzene; 3: |Wittig Olefination;
DOI:10.3987/COM-13-12905