ethyl 4-[3-(5-dimethylamino-naphthalene-1-sulfonylamino)propoxy]-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate

Base Information

Chemical Name:ethyl 4-[3-(5-dimethylamino-naphthalene-1-sulfonylamino)propoxy]-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate
CAS No.:870177-29-0
Molecular Formula:C₅₈H₉₆N₂O₂₃S
Molecular Weight:1221.47
Hs Code.:

Synonyms:ethyl 4-[3-(5-dimethylamino-naphthalene-1-sulfonylamino)propoxy]-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate

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Chemical Property of ethyl 4-[3-(5-dimethylamino-naphthalene-1-sulfonylamino)propoxy]-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate

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Technology Process of ethyl 4-[3-(5-dimethylamino-naphthalene-1-sulfonylamino)propoxy]-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate

There total 6 articles about ethyl 4-[3-(5-dimethylamino-naphthalene-1-sulfonylamino)propoxy]-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.3%

: ethyl 4-(trifluoroacetato-3-ammoniumpropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 870177-29-0
ethyl 4-[3-(5-dimethylamino-naphthalene-1-sulfonylamino)propoxy]-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/chem.200401078

Reference yield:

: 870177-06-3
ethyl 4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(benzyloxy)benzoate

: 870177-29-0
ethyl 4-[3-(5-dimethylamino-naphthalene-1-sulfonylamino)propoxy]-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / H₂ / Pd/C / methanol / 1 h

2: 65 percent / K₂CO₃ / dimethylformamide / 72 h / 80 °C

3: 91 percent / CH₂Cl₂ / 12 h / 20 °C

4: 99.3 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200401078

Reference yield:

: 831-61-8
Ethyl gallate

: 870177-29-0
ethyl 4-[3-(5-dimethylamino-naphthalene-1-sulfonylamino)propoxy]-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / KHCO₃; KI / dimethylformamide / 96 h / 20 °C

2: 65 percent / K₂CO₃ / dimethylformamide / 72 h / 80 °C

3: 91 percent / CH₂Cl₂ / 12 h / 20 °C

4: 99.3 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C

With potassium carbonate; potassium hydrogencarbonate; triethylamine; potassium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200401078