C₂₂H₁₇N₃O₃

Base Information

• Chemical Name: C₂₂H₁₇N₃O₃
• CAS No.: 1400683-62-6
• Molecular Formula: C₂₂H₁₇N₃O₃
• Molecular Weight: 371.395
• Mol file: 1400683-62-6.mol

Synonyms:C₂₂H₁₇N₃O₃

Chemical Property of C₂₂H₁₇N₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₁₇N₃O₃

There total 1 articles about C₂₂H₁₇N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

4-nitro-benzoyl chloride (122-04-3) + 5-phenyldipyrromethane (107798-98-1) → C22H17N3O3 (1400683-62-6)

Guidance literature:

5-phenyldipyrromethane; With isopropylmagnesium bromide; In tetrahydrofuran; toluene; for 0.333333h; Inert atmosphere; Cooling with ice;

4-nitro-benzoyl chloride; In tetrahydrofuran; toluene; at -78 - 20 ℃; for 1h; Inert atmosphere;

DOI:10.1021/ic3015354

Reference yield: 74.0%

C22H17N3O3 (1400683-62-6) → C22H16BrN3O3 (1400683-63-7)

Guidance literature:

With N-Bromosuccinimide; In tetrahydrofuran; at -78 ℃; for 1h;

DOI:10.1021/ic3015354

Reference yield:

C22H17N3O3 (1400683-62-6) → C34H25N5O2Zn (1400683-72-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide / tetrahydrofuran / 1 h / -78 °C

2.1: methanol / tetrahydrofuran / 0.75 h / Cooling with ice

2.2: 0.5 h

2.3: air / 24 h / 85 °C

With methanol; N-Bromosuccinimide; In tetrahydrofuran;

DOI:10.1021/ic3015354

upstream raw materials:

4-nitro-benzoyl chloride

5-phenyldipyrromethane

Downstream raw materials:

C₂₂H₁₆BrN₃O₃

C₃₄H₂₅N₅O₂Zn

C₃₆H₂₉N₅OZn