N-Benzyloxycarbonyl-γ-tert.-butyl-L-glutaminsaeure-pentachlor-phenyl-diester

Base Information

• Chemical Name: N-Benzyloxycarbonyl-γ-tert.-butyl-L-glutaminsaeure-pentachlor-phenyl-diester
• CAS No.: 6233-91-6
• Molecular Formula: C₂₃H₂₂Cl₅NO₆
• Molecular Weight: 585.696
• Mol file: 6233-91-6.mol

Synonyms:N-Benzyloxycarbonyl-γ-tert.-butyl-L-glutaminsaeure-pentachlor-phenyl-diester

Chemical Property of N-Benzyloxycarbonyl-γ-tert.-butyl-L-glutaminsaeure-pentachlor-phenyl-diester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-Benzyloxycarbonyl-γ-tert.-butyl-L-glutaminsaeure-pentachlor-phenyl-diester

There total 1 articles about N-Benzyloxycarbonyl-γ-tert.-butyl-L-glutaminsaeure-pentachlor-phenyl-diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Pentachlorophenol (87-86-5,67471-28-7) + methyl 2(S)-2-benzyloxycarbonylamino-4-tert-butoxycarbonylbutanoate (56877-41-9) → N-Benzyloxycarbonyl-γ-tert.-butyl-L-glutaminsaeure-pentachlor-phenyl-diester (6233-91-6)

Guidance literature:

Multistep reaction; (i) aq. NaOH, acetone, (ii) /BRN= 1285380/, DCC, CH₂Cl₂;

DOI:10.1021/ja00962a035

Reference yield:

N-Benzyloxycarbonyl-γ-tert.-butyl-L-glutaminsaeure-pentachlor-phenyl-diester (6233-91-6) → γ-tert.Butyl-L-glutaminsaeure-pentachlorphenylester

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; chloroform;

DOI:10.1021/ja00962a035

Reference yield:

N-Benzyloxycarbonyl-γ-tert.-butyl-L-glutaminsaeure-pentachlor-phenyl-diester (6233-91-6) → N-Benzyloxycarbonyl-γ-tert.butyl-L-glutamyl-L-alanin-pentachlorphenylester

Guidance literature:

Multi-step reaction with 2 steps

2: (i) (saponification), (ii) /BRN= 1285380/, DCC

DOI:10.1021/ja01079a021

upstream raw materials:

Pentachlorophenol

methyl 2(S)-2-benzyloxycarbonylamino-4-tert-butoxycarbonylbutanoate

Downstream raw materials:

N-benzyloxycarbonyl-γ-tert-butyl-L-glutamyl-L-alanine methyl ester

N-Benzyloxycarbonyl-γ-tert.-butyl-L-glutamyl-L-alanin-hydrazid