C₂₁H₁₇IO₃

Base Information

Chemical Name:C₂₁H₁₇IO₃
CAS No.:1415684-40-0
Molecular Formula:C₂₁H₁₇IO₃
Molecular Weight:444.269
Hs Code.:

C<sub>21</sub>H<sub>17</sub>IO<sub>3</sub>

Synonyms:C₂₁H₁₇IO₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₁₇IO₃

Chemical Property:

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Technology Process of C₂₁H₁₇IO₃

There total 2 articles about C₂₁H₁₇IO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 57772-57-3
5-hydroxy-2-iodo-benzoic acid

: 100-39-0
benzyl bromide

: 1415684-40-0
C₂₁H₁₇IO₃

Guidance literature:: With potassium carbonate; In acetone; for 5h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.10.092

Reference yield:

: 394-31-0
2-amino-5-hydroxybenzoic acid

: 1415684-40-0
C₂₁H₁₇IO₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / water / 5 °C

1.2: 0.17 h / 5 °C

1.3: 21 h / 5 - 100 °C

2.1: potassium carbonate / acetone / 5 h / Reflux

With sulfuric acid; potassium carbonate; In water; acetone;
DOI:10.1002/asia.201601183

Reference yield:

: 120-72-9
indole

: 1415684-40-0
C₂₁H₁₇IO₃

: 1415684-41-1
C₂₉H₂₃NO₃

Guidance literature:: indole; C₂₁H₁₇IO₃; With copper; potassium carbonate; In Triethylene glycol dimethyl ether; at 140 ℃; for 48h; Inert atmosphere;

With benzyl bromide; In Triethylene glycol dimethyl ether; at 20 - 140 ℃; for 15h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.10.092