2-benzoyl-4-bromobenzoic acid ethyl ester

Base Information

Chemical Name:2-benzoyl-4-bromobenzoic acid ethyl ester
CAS No.:1131040-47-5
Molecular Formula:C₁₆H₁₃BrO₃
Molecular Weight:333.181
Hs Code.:

Synonyms:2-benzoyl-4-bromobenzoic acid ethyl ester

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Chemical Property of 2-benzoyl-4-bromobenzoic acid ethyl ester

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Technology Process of 2-benzoyl-4-bromobenzoic acid ethyl ester

There total 1 articles about 2-benzoyl-4-bromobenzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 5798-75-4
Ethyl 4-bromobenzoate

: 98-88-4
benzoyl chloride

: 1131040-47-5
2-benzoyl-4-bromobenzoic acid ethyl ester

Guidance literature:: Ethyl 4-bromobenzoate; With bis(2,2,6,6-tetramethylpiperidin-1-yl)magnesium-bis(lithium chloride) complex; zinc(II) chloride; In tetrahydrofuran; at 25 ℃; for 12h; Inert atmosphere;

benzoyl chloride; With copper(l) cyanide; In tetrahydrofuran; at -40 - 25 ℃; Inert atmosphere;
DOI:10.1002/chem.200801558

Reference yield: 22.0%

: 1131040-47-5
2-benzoyl-4-bromobenzoic acid ethyl ester

: 75-31-0
isopropylamine

: 5-bromo-2-isopropyl-3-phenyl-2,3-dihydroisoindol-1-one

Guidance literature:: 2-benzoyl-4-bromobenzoic acid ethyl ester; isopropylamine; With titanium tetrachloride; In 1,2-dichloro-ethane; at 0 - 80 ℃; for 18h;

With sodium cyanoborohydride; In methanol; 1,2-dichloro-ethane; at 50 ℃;