3-Cyclohexen-1-ol,6-methyl-3-(1-methylethyl)-,(1R-cis)-(9CI)

Base Information

• Chemical Name: 3-Cyclohexen-1-ol,6-methyl-3-(1-methylethyl)-,(1R-cis)-(9CI)
• CAS No.: 162238-86-0
• Molecular Formula: C10H18 O
• Molecular Weight: 154.25
• Mol file: 162238-86-0.mol

Synonyms:3-Cyclohexen-1-ol,6-methyl-3-(1-methylethyl)-,(1R-cis)-(9CI)

Chemical Property of 3-Cyclohexen-1-ol,6-methyl-3-(1-methylethyl)-,(1R-cis)-(9CI)

Chemical Property:

• PSA: 20.23000
• LogP: 2.35960

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Cyclohexen-1-ol,6-methyl-3-(1-methylethyl)-,(1R-cis)-(9CI)

There total 1 articles about 3-Cyclohexen-1-ol,6-methyl-3-(1-methylethyl)-,(1R-cis)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

p-menth-4-en-2-one (142472-68-2,242127-32-8) → (1S,6S)-3-Isopropyl-6-methyl-cyclohex-3-enol (162238-85-9) + (1R,6S)-3-Isopropyl-6-methyl-cyclohex-3-enol (162238-86-0)

Guidance literature:

With potassium tri-sec-butyl-borohydride; In tetrahydrofuran; at -78 ℃; for 0.5h;

DOI:10.1021/jo00107a031

Reference yield: 83.0%

(1R,6S)-3-Isopropyl-6-methyl-cyclohex-3-enol (162238-86-0) + 3,5-dinitrobenoyl chloride (99-33-2) → 3,5-Dinitro-benzoic acid (1R,6S)-3-isopropyl-6-methyl-cyclohex-3-enyl ester

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 ℃; for 1.5h;

DOI:10.1021/jo00107a031

Reference yield:

R-(+)-α-trifluoromethyl-α-methoxy-phenylacetic acid (20445-31-2) + (1R,6S)-3-Isopropyl-6-methyl-cyclohex-3-enol (162238-86-0) → (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (1R,6S)-3-isopropyl-6-methyl-cyclohex-3-enyl ester

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; for 1h; Ambient temperature;

DOI:10.1021/jo00107a031

upstream raw materials:

p-menth-4-en-2-one