(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxy-N-(n-nonyl)cyclohexanamine

Base Information

Chemical Name:(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxy-N-(n-nonyl)cyclohexanamine
CAS No.:1371586-83-2
Molecular Formula:C₄₄H₅₇NO₅
Molecular Weight:679.94
Hs Code.:

Synonyms:(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxy-N-(n-nonyl)cyclohexanamine

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Chemical Property of (1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxy-N-(n-nonyl)cyclohexanamine

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Technology Process of (1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxy-N-(n-nonyl)cyclohexanamine

There total 3 articles about (1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxy-N-(n-nonyl)cyclohexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 124-19-6
nonan-1-al

: 1371586-78-5
(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxycyclohexanamine

: 1371586-83-2
(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxy-N-(n-nonyl)cyclohexanamine

Guidance literature:: With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jm300342q

Reference yield:

: 864948-63-0
(+)-(1R,2R,3S,4R,5R,6S)-2-azido-3,4,5,6-tetrakisbenzyloxycyclohexanol

: 1371586-83-2
(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxy-N-(n-nonyl)cyclohexanamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

3.1: sodium cyanoborohydride; acetic acid / methanol / 4 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium hydride; sodium cyanoborohydride; acetic acid; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jm300342q

Reference yield:

: 1371586-74-1
((1S,2R,3R,4S,5R,6R)-5-azido-6-methoxycyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

: 1371586-83-2
(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxy-N-(n-nonyl)cyclohexanamine

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2: sodium cyanoborohydride; acetic acid / methanol / 4 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium cyanoborohydride; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jm300342q