((1S,2R,3R,4S,5R,6R)-5-azido-6-methoxycyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

Base Information

Chemical Name:((1S,2R,3R,4S,5R,6R)-5-azido-6-methoxycyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene
CAS No.:1371586-74-1
Molecular Formula:C₃₅H₃₇N₃O₅
Molecular Weight:579.696
Hs Code.:

Synonyms:((1S,2R,3R,4S,5R,6R)-5-azido-6-methoxycyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

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Chemical Property of ((1S,2R,3R,4S,5R,6R)-5-azido-6-methoxycyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

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Technology Process of ((1S,2R,3R,4S,5R,6R)-5-azido-6-methoxycyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

There total 1 articles about ((1S,2R,3R,4S,5R,6R)-5-azido-6-methoxycyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 864948-63-0
(+)-(1R,2R,3S,4R,5R,6S)-2-azido-3,4,5,6-tetrakisbenzyloxycyclohexanol

: 74-88-4
methyl iodide

: 1371586-74-1
((1S,2R,3R,4S,5R,6R)-5-azido-6-methoxycyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

Guidance literature:: (+)-(1R,2R,3S,4R,5R,6S)-2-azido-3,4,5,6-tetrakisbenzyloxycyclohexanol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.25h;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;
DOI:10.1021/jm300342q

Reference yield: 95.0%

: 1371586-74-1
((1S,2R,3R,4S,5R,6R)-5-azido-6-methoxycyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

: 1371586-78-5
(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxycyclohexanamine

Guidance literature:: ((1S,2R,3R,4S,5R,6R)-5-azido-6-methoxycyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;

With water; sodium sulfate; In tetrahydrofuran;
DOI:10.1021/jm300342q

Reference yield:

: 1371586-74-1
((1S,2R,3R,4S,5R,6R)-5-azido-6-methoxycyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

: 1371586-83-2
(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-methoxy-N-(n-nonyl)cyclohexanamine

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2: sodium cyanoborohydride; acetic acid / methanol / 4 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium cyanoborohydride; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jm300342q