3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(4-methoxyphenyl)-1,2,4-oxadiazole

Base Information

Chemical Name:3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(4-methoxyphenyl)-1,2,4-oxadiazole
CAS No.:1312793-90-0
Molecular Formula:C₂₁H₂₂N₂O₄
Molecular Weight:366.417
Hs Code.:

Synonyms:3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(4-methoxyphenyl)-1,2,4-oxadiazole

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Chemical Property of 3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(4-methoxyphenyl)-1,2,4-oxadiazole

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Technology Process of 3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(4-methoxyphenyl)-1,2,4-oxadiazole

There total 3 articles about 3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(4-methoxyphenyl)-1,2,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₄N₂O₅

: 1312793-90-0
3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(4-methoxyphenyl)-1,2,4-oxadiazole

Guidance literature:: In N,N-dimethyl-formamide; at 110 ℃; for 10h; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.03.031

Reference yield:

: 159783-16-1
3-(cyclopentyloxy)-4-methoxybenzonitrile

: 1312793-90-0
3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(4-methoxyphenyl)-1,2,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine hydrochloride; sodium carbonate / ethanol; water / 18 h / 0 °C / Reflux

2.1: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

2.2: 3.5 h / 0 - 30 °C / Inert atmosphere

3.1: N,N-dimethyl-formamide / 10 h / 110 °C / Inert atmosphere

With hydroxylamine hydrochloride; sodium carbonate; dicyclohexyl-carbodiimide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.03.031

Reference yield:

: 874485-04-8
C₁₃H₁₈N₂O₃

: 100-09-4
4-methoxybenzoic acid

: 1312793-90-0
3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(4-methoxyphenyl)-1,2,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

1.2: 3.5 h / 0 - 30 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide / 10 h / 110 °C / Inert atmosphere

With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.03.031