6-Chloro-5-methylindoline

Base Information

Chemical Name:6-Chloro-5-methylindoline
CAS No.:162100-44-9
Molecular Formula:C₉H₁₀ClN
Molecular Weight:167.638
Hs Code.:
Mol file:162100-44-9.mol

Synonyms:6-Chloro-5-methyl-2,3-dihydro-1H-indole;6-Chloro-5-methyl-2,3-dihydroindole; 6-Chloro-5-methylindoline

Suppliers and Price of 6-Chloro-5-methylindoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
6-CHLORO-5-METHYL-2,3-DIHYDRO-1H-INDOLE 95.00%
5MG
$ 502.76

AK Scientific
6-Chloro-5-methyl-2,3-dihydro-1H-indole
100mg
$ 398.00

Total 8 raw suppliers

Chemical Property of 6-Chloro-5-methylindoline

Chemical Property:

PSA：12.03000
LogP:2.75440

Purity/Quality:

97% ^*data from raw suppliers

6-CHLORO-5-METHYL-2,3-DIHYDRO-1H-INDOLE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-Chloro-5-methylindoline

There total 8 articles about 6-Chloro-5-methylindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 162100-42-7
6-chloro-5-methyl-1H-indole

: 162100-44-9
6-chloro-5-methyl-2,3-dihydro-1H-indole

Guidance literature:: With sodium cyanoborohydride; acetic acid; for 3h; Ambient temperature;
DOI:10.1021/jm970741j

Reference yield:

: 71270-61-6
N-(3-chloro-4-methylphenyl)methanesulfonamide

: 162100-44-9
6-chloro-5-methyl-2,3-dihydro-1H-indole

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / dimethylformamide / 0 °C

2: TiCl₄ / toluene / 2 h

3: aq. NaOH / ethanol / 0.5 h / Heating

4: glac. AcOH, sodium cyanoborohydride / 3 h / Ambient temperature

With sodium hydroxide; titanium tetrachloride; sodium hydride; sodium cyanoborohydride; acetic acid; In ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm970741j

Reference yield:

: 95-74-9,827571-80-2
3-chloro-p-toluidine

: 162100-44-9
6-chloro-5-methyl-2,3-dihydro-1H-indole

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / CH₂Cl₂ / 2 h

2: NaH / dimethylformamide / 0 °C

3: TiCl₄ / toluene / 2 h

4: aq. NaOH / ethanol / 0.5 h / Heating

5: glac. AcOH, sodium cyanoborohydride / 3 h / Ambient temperature

With pyridine; sodium hydroxide; titanium tetrachloride; sodium hydride; sodium cyanoborohydride; acetic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm970741j