prop-2-yn-1-yl 1-bromo-2,2-diphenylcyclopropanecarboxylate

Base Information

Chemical Name:prop-2-yn-1-yl 1-bromo-2,2-diphenylcyclopropanecarboxylate
CAS No.:1335201-48-3
Molecular Formula:C₁₉H₁₅BrO₂
Molecular Weight:355.231
Hs Code.:

Synonyms:prop-2-yn-1-yl 1-bromo-2,2-diphenylcyclopropanecarboxylate

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Chemical Property of prop-2-yn-1-yl 1-bromo-2,2-diphenylcyclopropanecarboxylate

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Technology Process of prop-2-yn-1-yl 1-bromo-2,2-diphenylcyclopropanecarboxylate

There total 1 articles about prop-2-yn-1-yl 1-bromo-2,2-diphenylcyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 19481-83-5
1-bromo-2,2-diphenylcyclopropanecarboxylic acid

: 106-96-7
propargyl bromide

: 1335201-48-3
prop-2-yn-1-yl 1-bromo-2,2-diphenylcyclopropanecarboxylate

Guidance literature:: 1-bromo-2,2-diphenylcyclopropanecarboxylic acid; With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h; Inert atmosphere;

propargyl bromide; In N,N-dimethyl-formamide; toluene; at 20 ℃; for 19h; Inert atmosphere;
DOI:10.1021/ol202178t

Reference yield: 88.0%

: 1335201-48-3
prop-2-yn-1-yl 1-bromo-2,2-diphenylcyclopropanecarboxylate

: 1335201-50-7
prop-2-yn-1-yl 2-methyl-3,3-diphenylacrylate

Guidance literature:: With (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 40 ℃; for 8h; chemoselective reaction; Irradiation; Inert atmosphere;
DOI:10.1021/ol202178t