5,17-bis(phenylazo)-26,28-dihydroxy-25,27-di(ethoxycarbonylmethoxy)calix[4]arene

Base Information

Chemical Name:5,17-bis(phenylazo)-26,28-dihydroxy-25,27-di(ethoxycarbonylmethoxy)calix[4]arene
CAS No.:471281-97-7
Molecular Formula:C₄₈H₄₄N₄O₈
Molecular Weight:804.899
Hs Code.:

Synonyms:5,17-bis(phenylazo)-26,28-dihydroxy-25,27-di(ethoxycarbonylmethoxy)calix[4]arene

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Chemical Property of 5,17-bis(phenylazo)-26,28-dihydroxy-25,27-di(ethoxycarbonylmethoxy)calix[4]arene

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Technology Process of 5,17-bis(phenylazo)-26,28-dihydroxy-25,27-di(ethoxycarbonylmethoxy)calix[4]arene

There total 1 articles about 5,17-bis(phenylazo)-26,28-dihydroxy-25,27-di(ethoxycarbonylmethoxy)calix[4]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 369-57-3
benzenediazonium tetrafluoroborate

: 142267-55-8
25,27-bis[(ethoxycarbonyl)methoxy]-26,28-dihydroxycalix[4]arene

: 471281-97-7
5,17-bis(phenylazo)-26,28-dihydroxy-25,27-di(ethoxycarbonylmethoxy)calix[4]arene

Guidance literature:: With pyridine; In tetrahydrofuran; at 0 ℃; for 48h;
DOI:10.1016/S0040-4039(02)00690-1

Reference yield: 25.5%

: 105-36-2
ethyl bromoacetate

: 471281-97-7
5,17-bis(phenylazo)-26,28-dihydroxy-25,27-di(ethoxycarbonylmethoxy)calix[4]arene

: 5,17-bis(phenylazo)-25,26,27,28-tetra(ethoxycarbonylmethoxy)calix[4]arene

Guidance literature:: With sodium carbonate; In acetonitrile; for 72h; Heating;
DOI:10.1016/S0040-4039(02)00690-1

Reference yield:

: 471281-97-7
5,17-bis(phenylazo)-26,28-dihydroxy-25,27-di(ethoxycarbonylmethoxy)calix[4]arene

: 5,17-bis(phenylazo)-26,28-bis{[(ethoxycarbonyl)methylcarbamoyl]methoxy}-25,27-di(ethoxycarbonylmethoxy)calix[4]arene

Guidance literature:: Multi-step reaction with 2 steps

1: 25.5 percent / Na₂CO₃ / acetonitrile / 72 h / Heating

2: 33 percent / sodium carbonate; sodium iodide / acetonitrile / 72 h / Heating

With sodium carbonate; sodium iodide; In acetonitrile;
DOI:10.1016/S0040-4039(02)00690-1