5-<4-(2-bromoethyl)benzyl>-5-β-D-glucopyranosyl-1,3-dimethyl-5-(4-vinylbenzyl)barbiturate

Base Information

Chemical Name:5-<4-(2-bromoethyl)benzyl>-5-β-D-glucopyranosyl-1,3-dimethyl-5-(4-vinylbenzyl)barbiturate
CAS No.:160055-57-2
Molecular Formula:C₂₁H₂₇BrN₂O₈
Molecular Weight:515.358
Hs Code.:

Synonyms:5-<4-(2-bromoethyl)benzyl>-5-β-D-glucopyranosyl-1,3-dimethyl-5-(4-vinylbenzyl)barbiturate

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Chemical Property of 5-<4-(2-bromoethyl)benzyl>-5-β-D-glucopyranosyl-1,3-dimethyl-5-(4-vinylbenzyl)barbiturate

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Technology Process of 5-<4-(2-bromoethyl)benzyl>-5-β-D-glucopyranosyl-1,3-dimethyl-5-(4-vinylbenzyl)barbiturate

There total 3 articles about 5-<4-(2-bromoethyl)benzyl>-5-β-D-glucopyranosyl-1,3-dimethyl-5-(4-vinylbenzyl)barbiturate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 79050-33-2
4-(2-bromoethyl)-1-(bromomethyl)benzene

: 5-β-D-glucopyranosyl-1,3-dimethylbarbituric acid sodium salt

: 160055-57-2
5-<4-(2-bromoethyl)benzyl>-5-β-D-glucopyranosyl-1,3-dimethyl-5-(4-vinylbenzyl)barbiturate

Guidance literature:: With cetyltrimethylammonim bromide; In water; at 70 ℃; for 6h; Irradiation;
DOI:10.1016/0008-6215(94)84109-8

Reference yield:

: 2280-44-6
D-Glucose

: 160055-57-2
5-<4-(2-bromoethyl)benzyl>-5-β-D-glucopyranosyl-1,3-dimethyl-5-(4-vinylbenzyl)barbiturate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaHCO₃ / H₂O / 80 °C

2: 81 percent / hexadecyltrimethylammonium bromide / H₂O / 6 h / 70 °C / Irradiation

With cetyltrimethylammonim bromide; sodium hydrogencarbonate; In water;
DOI:10.1016/0008-6215(94)84109-8

Reference yield:

: 769-42-6
1,3-dimethylbarbituric acid

: 160055-57-2
5-<4-(2-bromoethyl)benzyl>-5-β-D-glucopyranosyl-1,3-dimethyl-5-(4-vinylbenzyl)barbiturate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaHCO₃ / H₂O / 80 °C

2: 81 percent / hexadecyltrimethylammonium bromide / H₂O / 6 h / 70 °C / Irradiation

With cetyltrimethylammonim bromide; sodium hydrogencarbonate; In water;
DOI:10.1016/0008-6215(94)84109-8