2-O-benzyl-1-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3-deoxy-2(S)-glycerol

Base Information

Chemical Name:2-O-benzyl-1-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3-deoxy-2(S)-glycerol
CAS No.:108811-13-8
Molecular Formula:C₃₇H₄₂O₇
Molecular Weight:598.736
Hs Code.:

Synonyms:2-O-benzyl-1-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3-deoxy-2(S)-glycerol

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Chemical Property of 2-O-benzyl-1-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3-deoxy-2(S)-glycerol

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Technology Process of 2-O-benzyl-1-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3-deoxy-2(S)-glycerol

There total 2 articles about 2-O-benzyl-1-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3-deoxy-2(S)-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84218-71-3,114079-12-8,127874-07-1,127875-24-5,127875-31-4,127875-37-0
4-O-acetyl-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 108811-13-8
2-O-benzyl-1-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3-deoxy-2(S)-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: carbon tetrabromide, triphenylphosphine / CH₂Cl₂

2: 1.) molecular sieves 4A, tetraethylammonium bromide / 2.) sodium methoxide / 1.) dichloroethane, 90 deg C, 24 h; 2.) methanol, 20 deg C, 6 h

With carbon tetrabromide; 4 A molecular sieve; tetraethylammonium bromide; triphenylphosphine; sodium methylate; In dichloromethane;

Reference yield:

: 94985-38-3
1-O-allyl-2-O-benzyl-3-deoxy-2(S)-glycerol

: 108811-13-8
2-O-benzyl-1-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3-deoxy-2(S)-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / palladium(II) chloride / methanol / 4 h / 20 °C

2: 1.) molecular sieves 4A, tetraethylammonium bromide / 2.) sodium methoxide / 1.) dichloroethane, 90 deg C, 24 h; 2.) methanol, 20 deg C, 6 h

With 4 A molecular sieve; tetraethylammonium bromide; palladium dichloride; sodium methylate; In methanol;

Reference yield: 95.0%

: 108811-13-8
2-O-benzyl-1-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3-deoxy-2(S)-glycerol

: 14227-66-8
acetobromocellobiose

: C₆₃H₇₆O₂₄

Guidance literature:: With 4 A molecular sieve; silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; 1.) -5 deg C, 4 h; 2.) 5-10 deg C, 16 h;