4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

Base Information

Chemical Name:4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate
CAS No.:858940-34-8
Molecular Formula:C₂₁H₂₈N₂O₅Si
Molecular Weight:416.549
Hs Code.:

Synonyms:4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

Suppliers and Price of 4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

There total 1 articles about 4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 131230-76-7
4-[(tert-butyldimethylsilyloxy)methyl]aniline

: 4457-32-3
4-nitrobenzyl chloroformate

: 858940-34-8
4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1016/j.bmc.2005.03.055

Reference yield: 75.0%

: 858940-34-8
4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

: 858940-35-9
4-nitrobenzyl 4-(hydroxymethyl)phenylcarbamate

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 0.25h;
DOI:10.1016/j.bmc.2005.03.055

Reference yield:

: 858940-34-8
4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

: 858940-36-0
4-({[(4-nitrobenzyl)oxy]carbonyl}amino)benzyl 4-nitrophenyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / hydrochloric acid / methanol / 0.25 h / 20 °C

2: 16 percent / ethyldiisopropylamine / tetrahydrofuran / 16 h / 20 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmc.2005.03.055