<2-<(2,6-dichloro-4-methoxyphenyl)amino>-5-methoxyphenyl>glyoxylic acid

Base Information

Chemical Name:<2-<(2,6-dichloro-4-methoxyphenyl)amino>-5-methoxyphenyl>glyoxylic acid
CAS No.:127792-39-6
Molecular Formula:C₁₆H₁₃Cl₂NO₅
Molecular Weight:370.189
Hs Code.:

Synonyms:<2-<(2,6-dichloro-4-methoxyphenyl)amino>-5-methoxyphenyl>glyoxylic acid

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Chemical Property of <2-<(2,6-dichloro-4-methoxyphenyl)amino>-5-methoxyphenyl>glyoxylic acid

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Technology Process of <2-<(2,6-dichloro-4-methoxyphenyl)amino>-5-methoxyphenyl>glyoxylic acid

There total 3 articles about <2-<(2,6-dichloro-4-methoxyphenyl)amino>-5-methoxyphenyl>glyoxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.3%

: 127792-38-5
1,3-dihydro-N-[(2,6-dichloro-4-methoxy)phenyl]-5-methoxy-2H-indole-2,3-dione

: 127792-39-6
<2-<(2,6-dichloro-4-methoxyphenyl)amino>-5-methoxyphenyl>glyoxylic acid

Guidance literature:: With sodium hydroxide; In ethanol; water; for 0.166667h; Heating;
DOI:10.1021/jm00171a008

Reference yield:

: 127792-36-3
4'-methoxy-2,6-dichloro-4-methoxydiphenylamine

: 127792-39-6
<2-<(2,6-dichloro-4-methoxyphenyl)amino>-5-methoxyphenyl>glyoxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / benzene / 2 h / Ambient temperature

2: 77.4 percent / AlCl₃ / various solvent(s) / 20 h / Ambient temperature

3: 87.3 percent / 1 N NaOH / ethanol; H₂O / 0.17 h / Heating

With sodium hydroxide; aluminium trichloride; In ethanol; water; benzene;
DOI:10.1021/jm00171a008

Reference yield:

: 127792-37-4
N-(4-methoxyphenyl)-N-(2',6'-dichloro-4'-methoxyphenyl)oxaniloyl chloride

: 127792-39-6
<2-<(2,6-dichloro-4-methoxyphenyl)amino>-5-methoxyphenyl>glyoxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 77.4 percent / AlCl₃ / various solvent(s) / 20 h / Ambient temperature

2: 87.3 percent / 1 N NaOH / ethanol; H₂O / 0.17 h / Heating

With sodium hydroxide; aluminium trichloride; In ethanol; water;
DOI:10.1021/jm00171a008