[(diphenylphosphino)methylene]diphenyl[(2,4,6-trimethylphenyl)methyl]phosphorane

Base Information

Chemical Name:[(diphenylphosphino)methylene]diphenyl[(2,4,6-trimethylphenyl)methyl]phosphorane
CAS No.:1372787-39-7
Molecular Formula:C₃₅H₃₄P₂
Molecular Weight:516.602
Hs Code.:

Synonyms:[(diphenylphosphino)methylene]diphenyl[(2,4,6-trimethylphenyl)methyl]phosphorane

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Chemical Property of [(diphenylphosphino)methylene]diphenyl[(2,4,6-trimethylphenyl)methyl]phosphorane

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Technology Process of [(diphenylphosphino)methylene]diphenyl[(2,4,6-trimethylphenyl)methyl]phosphorane

There total 2 articles about [(diphenylphosphino)methylene]diphenyl[(2,4,6-trimethylphenyl)methyl]phosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1372787-36-4
[(diphenylphosphino)methyl]diphenyl[(2,4,6-trimethylphenyl)methyl]phosphonium bromide

: 1372787-39-7
[(diphenylphosphino)methylene]diphenyl[(2,4,6-trimethylphenyl)methyl]phosphorane

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.3998/ark.5550190.0013.316

Reference yield:

: 4761-00-6
2,4,6-trimethylbenzylbromide

: 2071-20-7
bis-diphenylphosphinomethane

: 1372787-39-7
[(diphenylphosphino)methylene]diphenyl[(2,4,6-trimethylphenyl)methyl]phosphorane

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 48 h / 80 °C / Inert atmosphere

2: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With potassium tert-butylate; In tetrahydrofuran; toluene;
DOI:10.3998/ark.5550190.0013.316