exo-7,8-dibromo-5,10-epoxy-6,9-diphenyl-1,2,4b1,5,10,10a-hexahydrobenzo[k]cyclopenta[cd]fluoranthene

Base Information

Chemical Name:exo-7,8-dibromo-5,10-epoxy-6,9-diphenyl-1,2,4b1,5,10,10a-hexahydrobenzo[k]cyclopenta[cd]fluoranthene
CAS No.:1360548-22-6
Molecular Formula:C₃₄H₂₂Br₂O
Molecular Weight:606.356
Hs Code.:

Synonyms:exo-7,8-dibromo-5,10-epoxy-6,9-diphenyl-1,2,4b1,5,10,10a-hexahydrobenzo[k]cyclopenta[cd]fluoranthene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of exo-7,8-dibromo-5,10-epoxy-6,9-diphenyl-1,2,4b1,5,10,10a-hexahydrobenzo[k]cyclopenta[cd]fluoranthene

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Technology Process of exo-7,8-dibromo-5,10-epoxy-6,9-diphenyl-1,2,4b1,5,10,10a-hexahydrobenzo[k]cyclopenta[cd]fluoranthene

There total 1 articles about exo-7,8-dibromo-5,10-epoxy-6,9-diphenyl-1,2,4b1,5,10,10a-hexahydrobenzo[k]cyclopenta[cd]fluoranthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 6,7-dibromo-1,4-carbonylo-9,10-epoxy-1,2,3,4,5,8-hexaphenyl-1,4,4a,9,9a,10-hexahydroanthracene

: 23357-60-0
1,2-dihydropyracylene

: 1360548-22-6
exo-7,8-dibromo-5,10-epoxy-6,9-diphenyl-1,2,4b1,5,10,10a-hexahydrobenzo[k]cyclopenta[cd]fluoranthene

: 1360548-16-8
endo-7,8-dibromo-5,10-epoxy-6,9-diphenyl-1,2,4b1,5,10,10a-hexahydrobenzo[k]cyclopenta[cd]fluoranthene

Guidance literature:: In toluene; for 50h; Reflux;
DOI:10.1002/chem.201100443

Reference yield: 88.0%

: 1360548-22-6
exo-7,8-dibromo-5,10-epoxy-6,9-diphenyl-1,2,4b1,5,10,10a-hexahydrobenzo[k]cyclopenta[cd]fluoranthene

: 1360548-23-7
exo-7,8-dibromo-5,10-epoxy-6,9-diphenyl-4b1,5,10,10a-tetrahydrobenzo[k]cyclopenta[cd]fluoranthene

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; for 14h; Reflux;
DOI:10.1002/chem.201100443

Reference yield:

: 1360548-22-6
exo-7,8-dibromo-5,10-epoxy-6,9-diphenyl-1,2,4b1,5,10,10a-hexahydrobenzo[k]cyclopenta[cd]fluoranthene

: 1360548-25-9
exo-syn-5,12:7,10-diepoxy-6,11-diphenyl-4b,5,7,10,12,12a-hexahydrocyclopenta[cd]naphtho[2,3-k]fluoranthene

Guidance literature:: Multi-step reaction with 2 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 14 h / Reflux

2: n-butyllithium / hexane; toluene / 65 h / -30 - 20 °C / Inert atmosphere

With n-butyllithium; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In hexane; toluene;
DOI:10.1002/chem.201100443