[2-(8-Chloro-dibenzo[b,f]oxepin-10-ylsulfanyl)-ethyl]-methyl-carbamic acid phenyl ester

Base Information

Chemical Name:[2-(8-Chloro-dibenzo[b,f]oxepin-10-ylsulfanyl)-ethyl]-methyl-carbamic acid phenyl ester
CAS No.:72281-24-4
Molecular Formula:C₂₄H₂₀ClNO₃S
Molecular Weight:437.947
Hs Code.:

Synonyms:[2-(8-Chloro-dibenzo[b,f]oxepin-10-ylsulfanyl)-ethyl]-methyl-carbamic acid phenyl ester

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Chemical Property of [2-(8-Chloro-dibenzo[b,f]oxepin-10-ylsulfanyl)-ethyl]-methyl-carbamic acid phenyl ester

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Technology Process of [2-(8-Chloro-dibenzo[b,f]oxepin-10-ylsulfanyl)-ethyl]-methyl-carbamic acid phenyl ester

There total 5 articles about [2-(8-Chloro-dibenzo[b,f]oxepin-10-ylsulfanyl)-ethyl]-methyl-carbamic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 72281-15-3
2-chloro-11-[β-(dimethylamino)ethylthio]dibenz[b,f]oxepin

: 1885-14-9
phenyl chloroformate

: 72281-24-4
[2-(8-Chloro-dibenzo[b,f]oxepin-10-ylsulfanyl)-ethyl]-methyl-carbamic acid phenyl ester

Guidance literature:: With potassium carbonate; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1021/jm00179a005

Reference yield:

: 25563-04-6
o-(p-chlorophenoxy)phenylacetic acid

: 72281-24-4
[2-(8-Chloro-dibenzo[b,f]oxepin-10-ylsulfanyl)-ethyl]-methyl-carbamic acid phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 0.17 h / Heating

2: AlCl₃ / 1,2-dichloro-ethane / 2 h / Heating

3: boron trifluoride / acetic acid / 1.) RT, 16 h, 2.) reflux, 30 min

4: 65 percent / K₂CO₃ / CH₂Cl₂ / 24 h / Ambient temperature

With aluminium trichloride; thionyl chloride; boron trifluoride; potassium carbonate; In dichloromethane; acetic acid; 1,2-dichloro-ethane;
DOI:10.1021/jm00179a005

Reference yield:

: 25958-86-5
2-(4-chlorophenoxy)phenylacetonitrile

: 72281-24-4
[2-(8-Chloro-dibenzo[b,f]oxepin-10-ylsulfanyl)-ethyl]-methyl-carbamic acid phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / KOH / ethanol; H₂O / 3 h / Heating

2: thionyl chloride / 0.17 h / Heating

3: AlCl₃ / 1,2-dichloro-ethane / 2 h / Heating

4: boron trifluoride / acetic acid / 1.) RT, 16 h, 2.) reflux, 30 min

5: 65 percent / K₂CO₃ / CH₂Cl₂ / 24 h / Ambient temperature

With potassium hydroxide; aluminium trichloride; thionyl chloride; boron trifluoride; potassium carbonate; In ethanol; dichloromethane; water; acetic acid; 1,2-dichloro-ethane;
DOI:10.1021/jm00179a005