Technology Process of C22H28O8
There total 5 articles about C22H28O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dipyridinium dichromate;
In
dichloromethane;
at 0 - 20 ℃;
for 19h;
Molecular sieve;
Inert atmosphere;
DOI:10.1021/jm201131n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2,4,6-trimethyl-pyridine / dichloromethane / 1 h / -78 °C
2: dipyridinium dichromate / dichloromethane / 19 h / 0 - 20 °C / Molecular sieve; Inert atmosphere
With
2,4,6-trimethyl-pyridine; dipyridinium dichromate;
In
dichloromethane;
DOI:10.1021/jm201131n
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
1.2: 18 h / 20 °C / Inert atmosphere
2.1: acetic acid / water / 1 h / 20 °C
3.1: 2,4,6-trimethyl-pyridine / dichloromethane / 1 h / -78 °C
4.1: dipyridinium dichromate / dichloromethane / 19 h / 0 - 20 °C / Molecular sieve; Inert atmosphere
With
2,4,6-trimethyl-pyridine; dipyridinium dichromate; sodium hydride; acetic acid;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jm201131n