3,6-Dihydro-5-methyl-6-oxo-1,3-diphenyl-1-pyrimidinium-4-olat

Base Information

• Chemical Name: 3,6-Dihydro-5-methyl-6-oxo-1,3-diphenyl-1-pyrimidinium-4-olat
• CAS No.: 96807-23-7
• Molecular Formula: C₁₇H₁₄N₂O₂
• Molecular Weight: 278.31
• Mol file: 96807-23-7.mol

Synonyms:3,6-Dihydro-5-methyl-6-oxo-1,3-diphenyl-1-pyrimidinium-4-olat

Chemical Property of 3,6-Dihydro-5-methyl-6-oxo-1,3-diphenyl-1-pyrimidinium-4-olat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,6-Dihydro-5-methyl-6-oxo-1,3-diphenyl-1-pyrimidinium-4-olat

There total 3 articles about 3,6-Dihydro-5-methyl-6-oxo-1,3-diphenyl-1-pyrimidinium-4-olat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

(E)-N,N'-diphenylformimidamide (622-15-1,148651-26-7,149244-59-7,864131-95-3) + bis(2,4,6-trichlorophenyl) 2-methylmalonate (15781-71-2) → 3,6-Dihydro-5-methyl-6-oxo-1,3-diphenyl-1-pyrimidinium-4-olat (96807-23-7)

Guidance literature:

at 140 ℃; for 0.333333h;

Reference yield: 71.0%

bis(2,4,6-trichlorophenyl) 2-methylmalonate (15781-71-2) + N,N'-diphenylformamidine (864131-95-3) → 3,6-Dihydro-5-methyl-6-oxo-1,3-diphenyl-1-pyrimidinium-4-olat (96807-23-7)

Guidance literature:

Heating;

Reference yield:

2-isopropenylaniline (52562-19-3) + bis(2,4,6-trichlorophenyl) 2-methylmalonate (15781-71-2) + ethyl N-phenylformimidate (6780-49-0) → 3,6-Dihydro-5-methyl-6-oxo-1,3-diphenyl-1-pyrimidinium-4-olat (96807-23-7) + 3,6-Dihydro-1-(2-isopropenylphenyl)-5-methyl-6-oxo-3-phenyl-1-pyrimidinium-4-olat (112794-53-3)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given; 1) 20 h, 20 deg C, 2) 10 min, 140 deg C;

upstream raw materials:

(E)-N,N'-diphenylformimidamide

bis(2,4,6-trichlorophenyl) 2-methylmalonate

N,N'-diphenylformamidine

2-isopropenylaniline

Downstream raw materials:

1-Methyl-8,11-diphenyl-3-oxa-8,11-diazatricyclo<5.2.2.0^2,6>undecan-9,10-dion

3-Benzoyl-4-methyl-6,7-diphenyl-2,6,7-triazabicyclo<2.2.2>oct-2-en-5,8-dion

1-Methyl-8,11-diphenyl-2-piperidino-8,11-diazatricyclo<5.2.2.0^2,6>undecan-9,10-dion

3-Isopropylidene-1,6,7-triphenyl-2-oxa-6,7-diaza-bicyclo[2.2.2]octane-5,8-dione