(E)-3-cyclohexylacrylamide

Base Information

Chemical Name:(E)-3-cyclohexylacrylamide
CAS No.:22031-63-6
Molecular Formula:C₉H₁₅NO
Molecular Weight:153.224
Hs Code.:

Synonyms:(E)-3-cyclohexylacrylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-cyclohexylacrylamide

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Technology Process of (E)-3-cyclohexylacrylamide

There total 5 articles about (E)-3-cyclohexylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 683-72-7
dichloroacetamide

: 2043-61-0
cyclohexanecarbaldehyde

: 22031-63-6
(E)-3-cyclohexylacrylamide

Guidance literature:: With samarium; diiodomethane; In tetrahydrofuran; at 20 ℃; for 12h; optical yield given as %de;
DOI:10.1021/jo100320j

Reference yield: 57.0%

: 1597410-63-3
(E)-S-methyl 4-cyclohexyl-2-oxobut-3-enethioate

: 22031-63-6
(E)-3-cyclohexylacrylamide

Guidance literature:: With diphenylphosphoranyl azide; copper(II) bis(trifluoromethanesulfonate); In water; N,N-dimethyl-formamide; at 100 ℃; for 4h;
DOI:10.1021/acs.joc.7b03054

Reference yield:

: 4361-26-6
cyclohexyl-propiolic acid amide

: 22031-63-6
(E)-3-cyclohexylacrylamide

: 3-cyclohexylacrylamide

Guidance literature:: With potassium tert-butylate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In tetrahydrofuran; at 20 ℃; for 0.166667h; Overall yield = 35 percent; Overall yield = 30.8 mg; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.0c02567